The aim of this research is to synthesise carbon aerogels and to compare the differences in their textural, morphological and chemical properties when synthesised in basic and acidic media, and with two different types of pretreatment carbonization and activation with CO2. Four samples are prepared and characterised using TGA-DTA, SEM, DRX, isotherm determination of N2 adsorption-desorption at ...

ةیتوبكنعلا ةكبشلا و ينورتكللإا ثدحتلا و دیربلا لثم ةددعتملا اھتامدخب تینرتنلإا ةكبش ربتعت لا تامولعملا لدابت و لقنل ةیلاعف رثكلأا ةقیرط . يتلا تایوتحملاب ةمحدزم تدغ ةكبشلا هذھ نأ لاإ امداصت تببس " احضاو " امداصت لب اندیلاقت و انتاداع عم " نوناقلا عم . ةلیلق و ةئیذبلا عقاوملا ةیرصنعلا و ةیھاركلا ىلع عجشت يتلا عقاوملا و ةیحابلإا تایوتحملا تاذ ماشتحلاا لاإ تسیل يھ لافطلأا مھنمض نم و تینرتنلإا ةكبش...

A new semiorganic nonlinear optical crystal of bisthiourea nickel bromide (BTNB) was grown successfully by slow evaporation technique using water as solvent. The lattice parameters of the grown crystal have been determined by X-ray diffraction studies. Vibrational spectrum is recorded to determine symmetries of molecular vibrations. Optical absorbance spectrum recorded revealed that this crysta...

Tungstate exchanged Mg-Al layered double hydroxides as a recyclable heterogenised catalyst along with H2O2 as an oxidant for the oxidation of sec-amines to nitrones is developed for the first time, Reactions proceed at a fast rate in aqueous media in a single step at room temperature in good to excellent yields. The heterogenised catalyst showed higher activity (TOF) over their homogeneous anal...

Bismuth niobate solid solutions, BixNbOδ (2.5 ≤ x ≤ 6), have been prepared using a mechanochemical method. The solid solutions were also prepared using a solidstate conventional method for comparison purposes. Bi3NbO7 was successfully obtained via a mechanochemical method at a lower synthesis temperature (milled at 1000 rpm for one hour followed by heating at 700C for 24 h) than the conventiona...

In this research paper in air synthesis of Psyllium and zirconium(IV)tungstoiodophosphate based organo-inorganic hybrid ion exchanger has been reported. Synthesised hybrid ion exchanger has been characterized by FT-IR, SEM, EDS and TGA/DTA/DTG and chemical composition. Ion exchange capacity and thermal studies of the synthesised ion exchanger were investigated using the potassium chloride solut...

Recycled chicken eggshells after calcination have been used as a nonconventional heterogeneous catalyst for biodiesel synthesis from karanja oil from the pongam tree (Pongamia pinnata). The catalyst was characterized on X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, and differential thermal analysis/thermogravimetric analysis (DTA/TGA). The formation of the calcium oxi...

کچ ی هد هکبش هکبش رگسح یاه رگسح زا یا هنیزه مک و دودمح یژرنا اب ،کچوک یاه دنتسه یا یم شخپ رظن دروم هقطنم رد هک هداد ات دنوش عجم طیمح زا ار ییاه شزادرپ یارب و هدونم یروآ یزکرم هرگ هب ١ دننک لاسرا . م نینچهم ی هب و هداد صیخشت طیمح رد ار یدادخر عوقو دنناوت دنناسرب یزکرم هرگ علاطا . هکبش هنوگنیا ریخا یالهاس رد هنیمز رد اه یاهدربراک فلتمخ یاه هدرک ادیپ یدایز دنا . زا دنترابع اهدربراک نیا هلجم زا...

Abstract Pure ZnO and Cr-doped nanoparticles have been synthesized via a facile chemical co-precipitation route their structural, thermal characteristics were discussed systematically. In the experimental producer, doping concentration has varied range, 0.05–0.1 M, while calcined at 600 °C. The influence of Cr-doping on physical was investigated addressed. As-prepared samples analyzed XRD, FTIR...