We evaluated the evacuated phlebotomy tube designed specifically for trace metal analysis by Sherwood Medical Co. Pools of human serum containing known concentrations of aluminum, arsenic, calcium, cadmium, copper, chromium, iron, lead, magnesium, manganese, mercury, selenium, and zinc were exposed to the tube and rubber stopper for defined periods ranging from 5 min to 24 h. Analysis for each ...

V. F. Laurie, E. Villagra, J. Tapia, J. E. S. Sarkis, and Marcos A. Hortellani. 2010. Analysis of major metallic elements in Chilean wines by atomic absorption spectroscopy. Cien. Inv. Agr. 37(2): 77-85. A set of 75 wine samples from seven of the major wine producing regions in Chile were analyzed with flame atomic absorption spectroscopy (AAS) to determine their content of major metallic eleme...

Physio-chemical analysis of ash of Quercus infectoria, Cassia fistula, Tinospora cordifolia, Butea monosperma and Cedrela toona trees parts were carried out for present study. Atomic Absorption Spectroscopy (AAS) was used for quantitative estimation while chemical methods applied for qualitative estimation of minerals in plants ash. It is found that C. fistula, T. cordifolia, Q. infectoria and ...

Let’s say that you wanted to determine the heavy metal identities and concentrations in sediment and suspended solid samples obtained from present day Lake Nakuru. What technique would you use for this determination? You could use Atomic Absorption Spectroscopy (AAS) as was done in the article (Nelson 1998), but another technique, which is particularly good at detecting metals at the ppb level ...

lead, copper, cobalt, nickel, iron and zinc ions form monocitrate complexes (negative charge) in citrate solution which is absorbed on the citrate form of anion-exchange resins (citrate as counter ion) y exchange of citrate ion with citrate complexes. these are subsequently recovered from the resin by 0.5m ammonium citrate eluent at ph 2.0. under optimized conditions, quantitative recovery was ...

8-Hydroxyquinoline (8-HQ) was chosen as a powerful ligand for Hg solid phase extraction. Among several chelating resins based on 8-HQ, 5-phenylazo-8-hydroxyquinoline (5Ph8HQ) is used for mercury extraction in which the adsorption dynamics were fully studied. It has been shown that Hg(II) is totally absorbed by 5Ph8HQ within the first 30 minutes of contact time with t 1/2 5 minutes, following La...

This paper describes a novel approach for analysis of mercury speciation in fish using gas chromatography coupled with microwave-induced plasma optical emission spectrometry (GC-MIP-OES) in surfatron resonant cavity. Sample treatment was based on quantitative leaching of mercury species from fish tissue with ultrasound-assisted acidtoluene extraction. The extracted mercury species analyzed with...

An immobilized copper Schiff base tridentate complex was prepared in three steps from SBA-15 supports. The immobilized copper nanocatalyst (heterogeneous catalyst) was characterized by Fourier transform infrared spectroscopy (FT-IR), cross polarization magic angle spinning (CP-MAS), 13-carbon nuclear magnetic resonance (13C-NMR), atomic absorption spectroscopy (AAS), thermogravimetric analysis ...