نتایج جستجو برای: anthranilamide

تعداد نتایج: 59  

2015
Syunya Sasaki Matthew A. Lauber Darryl W. Brousmiche Zhengmao Hua Stephan M. Koza Ellen Guthrie Paula Magnelli Christopher H. Taron Kenneth J. Fountain

Conventional approaches to the preparation of N-glycans for HILICFLR-MS are either laborious, time-consuming, or require compromises in sensitivity. In the case of one of the most frequently employed labeling compounds, 2-aminobenzamide (2-AB), the resulting glycans can be readily detected by fluorescence but are difficult to detect by electrospray ionization mass spectrometry (ESI-MS). Variati...

Journal: :Analytical chemistry 2014
Stephane Houel Mark Hilliard Ying Qing Yu Niaobh McLoughlin Silvia Millan Martin Pauline M Rudd Jonathan P Williams Weibin Chen

Etanercept is a highly glycosylated therapeutic Fc-fusion protein that contains multiple N- and O-glycosylation sites. An in-depth characterization of the glycosylation of etanercept was carried out using liquid chromatography/mass spectrometry (LC/MS) methods in a systematic approach in which we analyzed the N- and O-linked glycans and located the occupied O-glycosylation sites. Etanercept was...

2014
Bing Shan Chunping Xu Yaoyang Zhang Tao Xu Joel M. Gottesfeld John R. Yates

Members of the 2-aminobenzamide class of histone deacetylase (HDAC) inhibitors show promise as therapeutics for the neurodegenerative diseases Friedreich's ataxia (FRDA) and Huntington's disease (HD). While it is clear that HDAC3 is one of the important targets of the 2-aminobenzamide HDAC inhibitors, inhibition of other class I HDACs (HDACs 1 and 2) may also be involved in the beneficial effec...

Journal: :Glycobiology 1998
K R Anumula S T Dhume

Facile labeling of oligosaccharides (acidic and neutral) in a nonselective manner was achieved with highly fluorescent anthranilic acid (AA, 2-aminobenzoic acid) (more than twice the intensity of 2-aminobenzamide, AB) for specific detection at very high sensitivity. Quantitative labeling in acetate-borate buffered methanol (approximately pH 5.0) at 80 degreesC for 60 min resulted in negligible ...

2015
Elisabetta Soragni C. James Chou James R. Rusche Joel M. Gottesfeld

The genetic defect in Friedreich's ataxia (FRDA) is the hyperexpansion of a GAA•TTC triplet in the first intron of the FXN gene, encoding the essential mitochondrial protein frataxin. Histone post-translational modifications near the expanded repeats are consistent with heterochromatin formation and consequent FXN gene silencing. Using a newly developed human neuronal cell model, derived from p...

2017
Christoph Kannicht Mario Kröning Barbara A. Solecka-Witulska Guido Kohla Julia Rosenlöcher

Prevention and treatment of bleeding in patients suffering from hemophilia A are inconvenient due to repeated intravenous infusions owing to the short half-life of coagulation factor VIII (FVIII) in circulation. Besides (glyco-)pegylation of the FVIII molecule, a bioengineering approach comprises the protein fusion to Fc-immunoglobulin (Ig)G that mediate protection from clearance or degradation...

Journal: :Plant physiology 2006
Teruko Konishi Hiroshi Ono Mayumi Ohnishi-Kameyama Satoshi Kaneko Tadashi Ishii

Arabinofuranosyltransferase activity was identified in Golgi membranes obtained from mung bean (Vigna radiata) hypocotyls. The enzyme transfers the arabinofuranosyl (Araf) residue from UDP-beta-L-arabinofuranose to exogenous (1, 5)-linked alpha-L-arabino-oligosaccharides labeled at their reducing ends with 2-aminobenzamide. The transferred residue was shown, using 1H-nuclear magnetic resonance ...

Journal: :Journal of medicinal chemistry 2009
Kenneth H Huang James M Veal R Patrick Fadden John W Rice Jeron Eaves Jon-Paul Strachan Amy F Barabasz Briana E Foley Thomas E Barta Wei Ma Melanie A Silinski Mei Hu Jeffrey M Partridge Anisa Scott Laura G DuBois Tiffany Freed Paul M Steed Andy J Ommen Emilie D Smith Philip F Hughes Angela R Woodward Gunnar J Hanson W Stephen McCall Christopher J Markworth Lindsay Hinkley Matthew Jenks Lifeng Geng Meredith Lewis James Otto Bert Pronk Katleen Verleysen Steven E Hall

A novel class of heat shock protein 90 (Hsp90) inhibitors was developed from an unbiased screen to identify protein targets for a diverse compound library. These indol-4-one and indazol-4-one derived 2-aminobenzamides showed strong binding affinity to Hsp90, and optimized analogues exhibited nanomolar antiproliferative activity across multiple cancer cell lines. Heat shock protein 70 (Hsp70) in...

Journal: :Glycobiology 2005
Baoyun Xia James A Royall Gautam Damera Goverdhan P Sachdev Richard D Cummings

Cystic fibrosis (CF) is the most lethal genetic disorder in Caucasians and is characterized by the production of excessive amounts of viscous mucus secretions in the airways of patients, leading to airway obstruction, chronic bacterial infections, and respiratory failure. Previous studies indicate that CF-derived airway mucins are glycosylated and sulfated differently compared with mucins from ...

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