Nanocomposite of NiAl2O4/SiO2 (NAS) was prepared through insitu solgel reaction, in which NiAl2O4 nanocrystals were dispersed in the silica glassy matrix. The prepared dried NAS gel, at 338 K, was heat treated to different temperature and identified the temperature range (1083 – 1163 K) of the nanocomposite formation through XRD patterns. From XRD patterns, crystallite size of NiAl2O4 particles...

we report the fabrication of pure CeO2, ZnO and SiO2 deposited CeO2 hybrid core-shell nanoparticles by simple and cost effective co precipitation method. The as synthesized samples were characterized by various experimental techniques such as XRD (X-ray diffraction), FTIR (Fourier Transform Infrared Spectroscopy) and HRTEM (High Field Transmission Tunneling Microscopy) measurements. XRD results...

A new high-pressure phase of U3O8, which has a fluorite-type structure, forms at pressures greater than 8.1 GPa that was confirmed by in situ x-ray diffraction (XRD) measurements. The fluorite-type U3O8 is stable at pressures at least up to 40 GPa and temperatures to 1700 K, and quenchable to ambient conditions. Based on the XRD analysis, there is a huge volume collapse (420%) for U3O8 during t...

tan films with different n2 partial pressure were deposited on 304 stainless steel using the magnetron sputtering method. the effect of gas pressure on the mechanical property, morphology and phase structure of the films is investigated by x-ray diffraction (xrd), atomic force microscopy (afm), microhardness testing, friction coefficient measurements, and wear mechanism study. the xrd results c...

Metal chelates of Schiff base derived from thiophene-2-aldehyde with 4-aminoantipyrine have been synthesized. The ligand and the complexes have been characterized by IR, molar conductance, magnetic moments, EPR, cyclic voltammetry, XRD and SEM measurements. Computational studies were also carried out. The geometry of the complexes was investigated by electronic spectral data and magnetic moment...

Micromachined nanocalorimetry sensors have shown excellent performance for hightemperature and high-scanning rate calorimetry measurements. Here we combine scanning AC nanocalorimetry with in-situ x-ray diffraction (XRD) to facilitate interpretation of the calorimetry measurements. Time-resolved XRD during in-situ operation of nanocalorimetry sensors using intense, high-energy synchrotron radia...

Ag2O/TiO2 nanobelt heterostructures have been found to possess high ultraviolet photocatalytic activity, but a poor cycling performance. After a S-doping treatment, the obtained Ag2O/Ag2S2O7/TiO2 heterostructured nanobelts exhibited an enhanced and stable photocatalytic activity under both ultraviolet and visible light irradiation, which was exemplified by photo-degradation of organic pollutant...

A combination of two analytical methods, time-resolved X-ray diffraction (XRD) and Raman spectroscopy, is presented as a novel tool for crystallization studies. An acoustic levitator was employed as sample environment. This setup enables the acquisition of XRD and Raman data in situ simultaneously within a 20 s period and hence permits investigation of polymorphic phase transitions during the c...

Hydration and dehydration reaction processes of many organic and inorganic compounds accompany phase changes, and X-ray diffraction (XRD) is a very powerful technique for studying the reaction processes. Thermal analysis is another important technique often used to obtain information needed for understanding the reaction processes. Commercially available instruments for XRD and thermal analysis...

Monoenergetic x-ray diffraction (XRD) analysis is an established standard for the assessment of urinary stone composition. The inherent low energy of x-rays used (8 keV), however, restricts penetration depth and imposes a requirement for small powdered samples. A technique capable of producing detailed information regarding component structural arrangements in calculi non-destructively would pr...