Positive-ion thermospray liquid chromatography-mass spectrometry (TSP-LC-MS) is used to detect organic acids via the direct injection of untreated urine from newborns and infants. Two methods are reported for the separation of organic acids. The separation of urinary organic acids is effected in either an acidic, pH 2.5 sulfuric acid, or a non-acidic, 0.05 M ammonium acetate, pH 6.8, mobile pha...

Sulfuric acid is a common chemical that is widely used in industry and is found in consumer products (e.g., car batteries, cleaning products). In the United States sulfuric acid is ranked number one in terms of production volume. Sulfur trioxide is a precursor to the production of sulfuric acid. Oleum (fuming sulfuric acid) is sulfur trioxide absorbed in concentrated sulfuric acid. Sulfur triox...

For the first time electron spin resonance (ESR) spectroscopic technique has been used for a highly selective determination of chlorpromazine. The method is based on the oxidation reaction of chlorpromazine with cerium(IV) in sulfuric acid media. In this method 3.8x10(-3) mol dm(-3) cerium(IV) was used in 0.035 mol dm(-3) sulfuric acid with the ESR spectra recorded at room temperature. A calibr...

In this work, thealkaline roasting and sulfuric acid leaching processes were employed to extract vanadium from the magnetite ore of Saghand mine in central Iran. The response surface methodology based on the central composite design model was applied to optimize the parameters involved in the processes. The studied roasting parameters were temperature (900-1100 °C), sodium carbonate percentage ...

Steam explosion is the most promising technology to replace conventional acid hydrolysis of lignocellulose for biomass pretreatment. In this paper, a new screw-steam-explosive extruder was designed and explored for xylose production and lignocellulose biorefinery at the pilot scale. We investigated the effect of different chemicals on xylose yield in the screw-steam-explosive extrusion process,...

In this paper, the corrosion behavior of the filled epoxy paint with the rice husk ash RHA on steel substrates in two different corrosive environments natural sea water and 2M sulfuric acid has been studied. Electrochemical impedance spectroscopy EIS was used to evaluate protective properties of different organic coating systems due to the different filler composition. RHA was prepared by heati...

The enzymatic degradation of chondroitin sulfuric acid can be catalyzed by purified bovine testicular hyaluronidase (1, 2) and by an enzyme preparation from Flavobacterium heparinum (3). Dodgson and Lloyd (4) obtained a chondroitinase from Proteus vulgaris that converted chondroitin sulfuric acid to the disaccharide, N-acetylchondrosin sulfate. Previous work from this laboratory (5) has confirm...

Biodiesel industry requires a cheaper and economical viable raw material that can replace the vegetable oil. Waste from animal and plant sources became the main option due the availability and cheap. In this study, coconut waste is used to produce biodiesel using methanol, acid sulfuric and KOH. In situ process is used, where all the catalyst, reagent and raw material is mixed together in one s...

0019-1035/$ see front matter Published by Elsevier doi:10.1016/j.icarus.2011.06.008 ⇑ Corresponding author. Fax: +1 301 286 0440. E-mail address: [email protected] (M.J. Loeffl We report laboratory studies on the 0.8 MeV proton irradiation of ices composed of sulfuric acid (H2SO4), sulfuric acid monohydrate (H2SO4 H2O), and sulfuric acid tetrahydrate (H2SO4 4H2O) between 10 and 180 K. Usin...