A method is described that accurately and rapidly quantifies the free and total phosphorous content of a commercially available, purified, phytic acid preparation. This allows its use as a standard for phytic acid determinations in foods. The method involves a wet ashing step followed by phosphorous measurement with a 1-amino-2-naphthol-4-sulfonic acid-molybdate reagent in a microplate reader a...

Two heteronuclear proton-carbon NMR experiments are applied to the DNA-octamer d(TTGGCCAA)2 with carbon in natural abundance. They lead to a complete assignment of the carbon resonances of the sugars and bases. In addition, several heteronuclear coupling constants, proton-carbon as well as proton-phosphorous and phosphorous-carbon, were determined. The information can be obtained in a reasonabl...

Communities of plants are thought to grow until they reach some limiting factor such as light, space, available nutrients or other limitation. Very often this limiting factor is a nutrient limitation. Therefore, if plants are provided with the essential nutrient they lack, they will expand their community’s biomass. This phenomenon is well studied in temperate communities. In those ecosystems, ...

This work examines the feasibility of liquid chromatography/mass spectrometry (LC/MS) time-of-flight (TOF) in conjunction with LC/MSD ion trap to analyze chloronicotinyl insecticides: acetamiprid, imidacloprid, and thiacloprid, in four salad vegetables: tomatoes, peppers, lettuce, and cucumbers. Included in this report are the LC/MSD TOF and LC/MSD Trap spectra of the three chloronicotinyl inse...

Recovering nutrients, especially phosphate resource, from wastewater have attracted increasing interest recently. Herein, an intermittently aerated membrane bioreactor (MBR) with a mesh filter was developed for simultaneous chemical oxygen demand (COD), total nitrogen (TN) and phosphorous removal, followed by phosphorus recovery from the phosphorus-rich sludge. This integrated system showed enh...

while the «classical insecticides» (ddt: dieldrin, malathion, etc.) mainly affect the adult stage of insects, dimilin belongs to a new group of insecticidal compounds that kills the insect in its larval stages, but has no lethal affect on the adult insect. its empirical formula is c14h9h2~f2cl. diflubenzuron is proposed as common name for the trade name dimilin. studies were made on c. pipiens,...

In vivo 31Phosphorous magnetic resonance spectroscopic imaging (31P MRSI) was performed on 18 chronic schizophrenic patients and 14 normal controls to determine if there was asymmetry of high-energy phosphorous metabolism in the temporal lobes of schizophrenic patients. Temporal lobe phosphorous metabolites were also correlated with severity of psychiatric symptomatology as assessed by the Brie...

Eleven schizophrenic patients and nine normal controls were studied using in vivo 31Phosphorous magnetic resonance spectroscopy (31P MRS) to test the hypothesis of metabolic asymmetry in the temporal lobes in schizophrenia. The controls did not demonstrate any asymmetry of phosphorous metabolite ratios, percentage of phosphorous metabolites, or pH. In the schizophrenics, however, phosphocreatin...

Agrochemical research over the last two decades has resulted in the discovery of chemically novel insecticides that mimic the action of the two insect growth and developmental hormones, the steroidal 20-hydroxyecdysone (20E) and the sesquiterpenoid juvenile hormone (JH). Bisacylhydrazines are non-steroidal agonists of 20E and exhibit their insecticidal activity via interaction with the ecdyster...