OBJECTIVE To assess four different chemical surface conditioning methods for ceramic material before bracket bonding, and their impact on shear bond strength and surface integrity at debonding. METHODS Four experimental groups (n = 13) were set up according to the ceramic conditioning method: G1 = 37% phosphoric acid etching followed by silane application; G2 = 37% liquid phosphoric acid etch...

highly self-ordered alumina nanopore arrays were fabricated using hard anodization technique in different mixtures of oxalic/phosphoric acid. the phosphoric acid concentration was varied from 0.05 to 0.3 m while the oxalic acid concentration was changed between 0.3 and 0.4 m. the self ordered nanoporous arrays were obtained in anodization voltage changing from 130 to 200 v. the interpore distan...

Introduction: The aim of this study was to compare the microleakage of beneath the orthodontic brackets bonded with 3 different bonding techniques and evaluate the effect of thermocycling. Methods: One hundred and twenty premolars were randomly divided into 6 groups, received the following treatment: group 1: 37% phosphoric acid gel+Unite primer+Unite adhesive, group 2: 37% phosphoric acid gel+...

A high performance liquid chromatography method was studied for determination of 18 ?-glycyrrhetinic acid in Glycyrrhiza glabra L. (licorice) extract. The operating condition were C-18 reversed phase column (VP-ODS, (250×4.6 mm, 5 mm)) at room temperature, acetonitril/phosphoric acid (3/1) as mobile phase, at flow rate of 0.6ml/min (0-8min), 0.4ml/min (8-20min) and UV detection at 230 nm. The...

Highly self-ordered alumina nanopore arrays were fabricated using hard anodization technique in different mixtures of oxalic/phosphoric acid. The phosphoric acid concentration was varied from 0.05 to 0.3 M while the oxalic acid concentration was changed between 0.3 and 0.4 M. The self ordered nanoporous arrays were obtained in anodization voltage changing from 130 to 200 V. The interpore distan...

Phosphoric acid monoesters are among the most important substances in materials chemistry, medicinal chemistry, and so on. Many phosphoric acid monoesters have been synthesized on an industrial scale and are used as necessities in our daily life. From the perspective of green chemistry, the direct catalytic condensation of equimolar amounts of phosphoric acid and alcohols is attractive for the ...

The purpose of this study was to establish an acid-etching procedure for altering the Ca/P ratio of the nanostructured surface of hydroxyapatite (HAP) by using surface chemical and morphological analyses (XPS, XRD, SEM, surface roughness, and wettability) and to evaluate the in vitro response of osteoblast-like cells (MC3T3-E1 cells) to the modified surfaces. This study utilized HAP and HAP tre...