نتایج جستجو برای: neutron diffraction analysis

تعداد نتایج: 2907556  

2009
J. Repper T. Keller M. Hofmann W. Petry E. Werner

The Neutron Larmor diffraction method is applied for the first time to determine absolute lattice spacing of a Silicon powder and polycrystalline IN718 samples. The absolute value of lattice spacing can be measured to an accuracy of 7· 10A. However, absolute determination of the lattice parameter is limited by the quality of the reference specimen used. Absolute lattice spacing determined by La...

Journal: :Physical review letters 2015
D H Torchinsky H Chu L Zhao N B Perkins Y Sizyuk T Qi G Cao D Hsieh

We report a global structural distortion in Sr_{2}IrO_{4} using spatially resolved optical second and third harmonic generation rotational anisotropy measurements. A symmetry lowering from an I4_{1}/acd to I4_{1}/a space group is observed both above and below the Néel temperature that arises from a staggered tetragonal distortion of the oxygen octahedra. By studying an effective superexchange H...

Journal: :Physical review. E, Statistical, nonlinear, and soft matter physics 2003
A Cailliaux C Alba-Simionesco B Frick L Willner I Goncharenko

This communication presents a determination of the glass transition of polybutadiene under very high pressure, and raises the problem of the determination of the relative effects of temperature and density on the glass transition, depending on the pressure and temperature conditions. Local structure and slow dynamics were studied, by neutron scattering and calorimetry. To the best of our knowle...

2017
Aline Dellicour Benedicte Vertruyen Mark O. Rikel Luca Lutterotti Alain Pautrat Bachir Ouladdiaf Daniel Chateigner

We describe how the contribution of crystallographic texture to the anisotropy of the resistivity of polycrystalline samples can be estimated by averaging over crystallographic orientations through a geometric mean approach. The calculation takes into account the orientation distribution refined from neutron diffraction data and literature values for the single crystal resistivity tensor. The e...

Journal: :Journal of Applied Physics 1998

2016
A. Berenov F. Le Goupil N. Alford

A series of Ba1-x-ySrxCayTiO3 compounds were prepared with varying average ionic radii and cation disorder on A-site. All samples showed typical ferroelectric behavior. A simple empirical equation correlated Curie temperature, TC, with the values of ionic radii of A-site cations. This correlation was related to the distortion of TiO6 octahedra observed during neutron diffraction studies. The eq...

Journal: :Physical review letters 2015
Steven M Disseler Julie A Borchers Charles M Brooks Julia A Mundy Jarrett A Moyer Daniel A Hillsberry Eric L Thies Dmitri A Tenne John Heron Megan E Holtz James D Clarkson Gregory M Stiehl Peter Schiffer David A Muller Darrell G Schlom William D Ratcliff

We report on the magnetic structure and ordering of hexagonal LuFeO_{3} films of variable thickness grown by molecular-beam epitaxy on YSZ (111) and Al_{2}O_{3} (0001) substrates. These crystalline films exhibit long-range structural uniformity dominated by the polar P6_{3}cm phase, which is responsible for the paraelectric to ferroelectric transition that occurs above 1000 K. Using bulk magnet...

2016
Orest Pavlosiuk Dariusz Kaczorowski Xavier Fabreges Arsen Gukasov Piotr Wiśniewski

We observed the coexistence of superconductivity and antiferromagnetic order in the single-crystalline ternary pnictide HoPdBi, a plausible topological semimetal. The compound orders antiferromagnetically at TN = 1.9 K and exhibits superconductivity below Tc = 0.7 K, which was confirmed by magnetic, electrical transport and specific heat measurements. The specific heat shows anomalies correspon...

Journal: :Physical chemistry chemical physics : PCCP 2011
Andrew S Powell Zlatka Stoeva Ronald I Smith Duncan H Gregory Jeremy J Titman

A combined NMR and neutron diffraction study has been carried out on three Li(3-x-y)Cu(x)N materials with x=0.17, x=0.29 and x=0.36. Neutron diffraction indicates that the samples retain the P6/mmm space group of the parent Li(3)N with Cu located only on Li(1) sites. The lattice parameters vary smoothly with x in a similar fashion to Li(3-x-y)Ni(x)N, but the Li(2) vacancy concentration for the ...

Journal: :Organic & biomolecular chemistry 2012
Fabrizio Fabris Ottorino De Lucchi Ilaria Nardini Marco Crisma Andrea Mazzanti Sax A Mason Marie-Hélène Lemée-Cailleau Francesca A Scaramuzzo Cristiano Zonta

(+)-syn-Benzotriborneol forms stable complexes with one molecule of water. This is due to the ability of the host to form three hydrogen bonds with water, to act simultaneously as a hydrogen-bond acceptor and donor, and to a perfect geometrical match between the pair. We report experimental (X-ray and neutron diffraction, VT NMR, DSC, TGA) and stereochemical studies carried out to elucidate and...

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