new two nano- sized schiff base complexes [m(l)], where l= 2, 2'-((1e, 1e')-(1, 2 phenylen bis (azanylylidene)) bis (methanylylidene)) bis (4-bromo phenolato) and m=cu or zn, (a, b complexes) were synthesized by ultrasonic irradiation. these complexes were characterized by elemental analysis, molar conductivity, ft-ir, fluorescence emission, 1h nmr, field emission scanning electron sp...

The SDS, PEG and CTAB roofed MgO nano powders were synthesized by co-precipitation method.  The sintered nano powders was shown Fm-3m space group with cubic phase obtained by the XRD pattern. The lattice strain was calculated to be used Williamson-Hall equations (W-H). The formation of Mg-O bond and hydroxyl radicals on the surface were confirmed by the FTIR analyses. The TEM revealed that the ...

We report on a possibility of efficient engineering of the acoustic phonon energy spectrum in multishell tubular structures produced by a novel high-tech method of self-organization of microand nano-architectures. The strain-driven roll-up procedure paved the way for novel classes of metamaterials such as single semiconductor radial microand nano-crystals and multi-layer spiral microand nano-su...

Filamentous networks can be widely found in biomaterials at the microand nano-scales. Some conventional theories may not apply to the materials with dimension at the microor nano-scale. The effects of strain gradient at the micro-meter scale and the effects of surface elasticity and initial stresses/strains at the nano-scale are incorporated into the deformation mechanisms in the analysis of st...

The development of new materials and devices for flexible electronics depends crucially on the understanding of how strain affects electronic material properties at the nano-scale. Scanning Kelvin-Probe Microscopy (SKPM) is a unique technique for nanoelectronic investigations as it combines non-invasive measurement of surface topography and surface electrical potential. Here we show that SKPM i...

Magnesium is an attractive hydrogen storage candidate due to its high gravimetric and volumetric capacities (7.6 wt.% 110 gH2/l, respectively). Unfortunately, use as a material for hampered by the stability of hydride, dissociation temperature 573–673 K slow reaction kinetics. In order overcome those drawbacks, important advancement toward controlling enthalpy desorption temperatures nano-struc...

Mechanical behavior of crystals is dictated by dislocation motion in response to applied force. While it is extremely difficult to directly observe the motion of individual dislocations, several correlations can be made between the microscopic stress-strain behavior and dislocation activity. Here, we present for the first time the differences observed between mechanical behavior in two fundamen...

a nano/ultra-fine grain al-0.2wt% zr alloy was produced by accumulated roll bonding (arb) processafter 10 cycles. the fraction of high angle grain boundaries increased from 8% to 65.4% during 10passes during arb process. this alloy was subjected to tensile test at different temperatures (523,573and 623 k) and strain rates (0.1 and 0.01 s-1). the optimum condition of temperature and strain rate ...