Ni(Mg)Al-layered hydroxides with molar ratios of (Ni + Mg)/Al = 2, 3, 4 and Ni/(Ni Mg) 0.1, 0.3, 0.5, 0.7 were synthesized by mechanochemical activation. It has been proven that the phase composition samples was presented a single hydrotalcite up to 0.5. For first time, catalysts based on prepared route have studied in reaction furfural hydrogenation. The correlation between conversion, selecti...