نتایج جستجو برای: limn2o4
تعداد نتایج: 298 فیلتر نتایج به سال:
Materials synthesis often provides opportunities for innovation. We demonstrate a general low-temperature (260°C) molten salt electrodeposition approach to directly electroplate the important lithium-ion (Li-ion) battery cathode materials LiCoO2, LiMn2O4, and Al-doped LiCoO2. The crystallinities and electrochemical capacities of the electroplated oxides are comparable to those of the powders sy...
We present inelastic neutron scattering results on [email protected]#O3.94 for temperatures T between 4 K and 295 K. We find that this compound is a charge-disordered material, in which both Mn-Mn and Mn-Mn nonlinear chains are formed once the electrons have become localized. Unlike the case for the parent material LiMn2O4, we find that the Jahn-Teller active Mn 31 ions in the Li-doped system are...
Porous nanostructured spinel LiMn2O4 has been successfully synthesized using a glycine-nitrate combustion process. The average primary particle size of the as-synthesized powders was about 10 nm, but increased to about 100 nm with improved crystallinity after calcination at 800 jC for 2 h. Yet, the calcined powders were still highly porous and displayed reversible capacity of about 112 mA h g 1...
limn2o4 spinel cathode materials have been successfully synthesized by solid-state reaction. surface of these particles were modified by nanostructured lifepo4 via sol gel dip coating method. synthesized products were characterized by thermally analyzed by thermogravimetric and differential thermal analysis(tg/dta), x-ray diffraction (xrd), scanning electron microscopy (sem), and energy dispers...
Powder neutron diffraction has been used to study the nature of the structural transition away from the Fd3m cubic structure upon cooling below ∼285 K in the spinel LiMn2O4. We report powder data taken between 10 K and 333 K and propose a large cell tetragonal structure in space group I41/amd for the material at 100 K. While complete segregation of the Mn3+ and Mn4+ ions is not possible in this...
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