نتایج جستجو برای: heating up solution synthesis

تعداد نتایج: 1769533  

The synthesis of nanocrystalline Fe3Al powder by mechanical alloying as well as the structural ordering of the synthesized Fe3Al particles during the subsequent thermal analysis were investigated. Mechanical alloying was performed up to 100 hours using a planetary ball mill apparatus with rotational speed of 300 rpm under argon atmosphere at ambient temperature. The synthesized powders were cha...

2004
Massimo Giovannini

Self-dual string cosmological models provide an effective example of bouncing solutions where a phase of accelerated contraction smoothly evolves into an epoch of decelerated Friedmann–Robertson–Walker expansion dominated by the dilaton. While the transition to the expanding regime occurs at sub-Planckian curvature scales, the Universe emerging after the bounce is cold, with sharply growing gau...

Journal: :Chemical communications 2014
Timothy H Vo Mikhail Shekhirev Donna A Kunkel François Orange Maxime J-F Guinel Axel Enders Alexander Sinitskii

Large quantities of narrow graphene nanoribbons with edge-incorporated nitrogen atoms can be synthesized via Yamamoto coupling of molecular precursors containing nitrogen atoms followed by cyclodehydrogenation using Scholl reaction.

Journal: :Jurnal kimia riset 2023

Microwaves have been used in various organic synthesis applications. The use of microwaves provides many advantages, including relatively short start-up and heating times, energy efficiency process costs, easy precise control, selective heating, better final product quality, improved dry material quality. were this study to convert chitin into chitosan determine the effect deacetylation time on...

2012
Vittorio Berbenni Chiara Milanese Giovanna Bruni Amedeo Marini

The synthesis of barium metastannate, BaSnO3, by heating mixtures of metal oxalates, either physically mixed or subjected to a phase of mechanical activation, up to temperatures in the range 750– 1200 ◦C has been studied. Simultaneous thermogravimetric-differential scanning calorimetric (TGDSC) analyses and powder X-ray diffractometry have been applied to check the advancement of the reactions....

2004
Geoffrey A. Tompsett Curtis Conner

Microwave zeolite synthesis has been shown to greatly reduce crystallization time. Although, fast efficient syntheses and quality crystalline products are widely reported(1), the mechanism leading to the formation of zeolites under microwave heating is not fully understood. Cundy(1) has reviewed the literature and concludes that the likely processes specific to microwave synthesis of zeolites a...

This paper focused on a simple approach for synthesis of molybdenum oxide (MoO3) nanoparticles and reports a facile route for synthesis of such nanoparticles, using microwave irradiation as a homogenous and powerful source of heating, using ethylene glycol as the solvent and heating medium. For more investigations, besides microwave heating, the obtained solutions were also treated by conventio...

E.C. Abdullah J.N. Sahu, Mubarak N. Mujawar,

Novel magnetic biochar has been successfully synthesized by using microwave technique, using discarded materials such as Empty Fruit Bunch (EFB). The optimized conditions for the best novel magnetic biochar synthesis are at 900 w reaction power, 20 min reaction time, and impregnation ratio 0.5 (biomas:FeCl3) The details physical and chemical analyses of novel magnetic biochar wer...

M. R. Aboutalebi, M. Reza Afshar, S. Ghafurian, S. H. Seyedein,

Abstract: Microwave processing is one of the novel methods for combustion synthesis of intermetallic compounds andcomposites. This method brings about a lot of opportunities for processing of uniquely characterized materials. In thisstudy, the combustion synthesis of TiAl/Al2O3 composite via microwave heating has been investigated by thedevelopment of a heat transfer model including a microwave...

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