AIM The purpose of this study was to characterise the enamel surface of sound deciduous teeth in terms of morphology, chemical composition, structure and crystalline phases. MATERIALS AND METHODS The enamel of 30 human deciduous teeth was examined by: Scanning Electron Microscopy (SEM), Energy Dispersive X-Ray Spectroscopy (EDS), X-ray Powder Diffraction (XRD), Fourier Transform Infrared Spec...

In this study, VA-CNTs were synthesized homogeneously on Al foil at 610 oC temperature by Floating Catalyst Chemical Vapor Deposition (FCCVD) method in a horizontal tube furnace. While ethanol was used as the carbon source, ferrocene catalyst. with diameters range of ~10-15 nm and lengths ~30-35 µm obtained. Structural morphological analyzes determined using X-Ray Diffraction (XRD), Field Emiss...

In this paper, the effect of magnetic field on the morphology, structure and magnetic properties of electrodeposited FeCu/Cu thin films was investigated. The films were deposited on Au2PdAg/glass substrates using electrodeposition technique in potentiostatic control. The magnetic fields of 5000 and 7000 Oe were applied on deposition bath during deposition. Two series of thin films were prepared...

Montmorillonite/ZrO2 nanocomposites were prepared by the sol-gel method underultrasonic irradiation. The montmorillonite was incorporated into Zirconium gel. After stirring for 24 hr, the mixture was irradiated for 30 min under ultrasonic irradiation. The filtrated composite gel was calcinated at 400°C for 3h in furnace. The morphology of prepared catalysts was characterized by field emis...

X-ray emission spectroscopy is widely used as a practical tool for compositional analysis of local specimen area and elemental mapping analysis in electron microscopes. X-rays with energy more than a few keV are dominantly due to electronic transitions between inner-shell electron levels. Those characteristic X-ray energies are useful for assignment of elements. On the other hand, X-rays origin...

This paper presents the chemical and physical characterizations of SiO 2 and SiO 2 -CaO bioactive glasses incorporated with samarium atoms, produced by sol-gel synthesis. The objective is to provide biocompatible and biodegradable radioactive seeds as an alternative to be used in Brachytherapy for the treatment of prostate cancer. The glasses were produced and analyzed by X-ray fluorescence spe...

Magnetic-fluorescent lanthanide doped sodium lutetium fluoride (NaLuF4:Yb3+/Er3+/Gd3+) nanocrystals were synthesized via facile hydrothermal method by varying concentration of Gd3+. Powder X-ray powder diffraction (PXRD), scanning electron microscopy (SEM),transmission electron microscopy (TEM), energy dispersive X-ray spectroscopy (EDS), p...

Un-doped and Cd-doped ZnZrO3/ZnO/ZrO2 nano composites (CDZZ-NCPs) (CD0-4) were synthesized by the hydrothermal method. The nano composites were characterized by various techniques such as Fourier Transform Infra-Red spectroscopy (FT-IR), X-ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FE-SEM) and Energy Dispersive X-Ray Analysis (EDS). The photocatalytic properties of CDZZ...

In this study, we reported a facile synthesis of bimetallic FeCo nanoparticles (Fe-Co NPs) by FeSO4.7H2O and Co(Ac)2.4H2O in the presence of sodium borohydride and 2-thiotic acid. The structure and morphology of the nanoparticles were characterized by X-Ray Diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDS), and Transmission Electron Micros...

For elemental analysis with energy dispersive X-ray spectroscopy (EDS) in transmission electron microscopy (TEM), the demand for the improved efficiency of X-ray detection, a higher counting rate, is very strong, because the improvement not only results in high throughput, but also extends the method to the specimens fairly susceptible to electron beam damage. We have already developed and intr...