Ultrashort pulsed lasers continue to see expanded application in many technologies such as microelectronics and precision manufacturing. The extremely short time duration (picosecond to femtosecond time scales) of these laser pulses create extremely non-equilibrium conditions during the heating and ablation of target materials. The result is generally efficient machining with little to no heat ...

In conjunction with microstructural interpretation, variation of the Sr/Ca ratio in otoliths of Platycephalus bassensis have been determined in an effort to uncover the role of biomineralisation in otolith trace element uptake. After subsequent microstructural analysis by Electron Backscatter Diffraction (EBSD), Sr/Ca ratios across otolith growth rings were determined by Electron Probe Microana...

In this study an advanced method for investigation of the microstructure such as electron backscatter diffraction (EBSD) together with in-situ tensile test in a scanning electron microscope (SEM) has been used at room temperature and 300°C. EBSD analyses provide information about crystallographic orientation in the microstructure and dislocation structures caused by deformation. The in-situ ten...

Imaging magnetic domains for soft magnetic materials using scanning electron microscopy (SEM) typically requires a specially modified setup. These modifications can include higher beam acceleration voltages, modifications of the sample and detector geometry, and/or specialized detectors to detect the spin polarization of secondary electrons [1,2]. In this research, a method is presented for ima...

Glass-ceramics grown from a glass of the composition Sr2TiSi2.45O8.9 (STS 45) are analyzed by scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). Oriented nucleation with the c-axes preferably perpendicular to the surface is detected. A very strong 001-texture is observed after only 10 μm of growth into the bulk, making this the first system in which an orientation p...

The focus of this study is the degradation of a near pearlitic microstructure under combined mechanical and thermal loadings leading to changes in mechanical properties. More specifically, it is examined how the orientation gradients inside the pearlite colonies, affect the spheroidisation. Samples were extracted from virgin near pearlitic railway wheels and prestrained, thereafter heat treated...

The electrodeposition of germanium at elevated temperatures up to 180 °C and pressures was studied from the ionic liquids 1-butyl-1-methylpyrrolidinium dicyanamide and 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide containing [GeCl4(BuIm)2] (where BuIm = 1-butylimidazole) or GeCl4. Cyclic voltammetry (CV), electrochemical quartz crystal microbalance (EQCM), rotating ring-disk e...

The different shot peening responds of a grey cast iron (GI) with its flake graphite and a compacted cast iron (CGI) with its vermicular graphite was analyzed and compared in this paper. For peening using identical parameters, CGI showed a larger plastic deformation zone with higher subsurface compressive stresses than GI. Electron backscatter diffraction (EBSD) mapping and backscatter electron...

The causes of liquation cracking in the heat-affected zone (HAZ) of a cast Mar-M004 superalloy weld were investigated. X-ray diffraction (XRD), electron probe microanalyzer (EPMA), and electron backscatter diffraction (EBSD) were applied to identify the final microconstituents at the solidification boundaries of the cast alloy. Fine borides and lamellar eutectics were present in front of some γ...