A series of copper oxide (CuOx) catalysts supported by oxidized multi-walled carbon nanotubes (OMWNT’s) were prepared by the wet impregnation method for the low temperature (200 °C) selective catalytic reduction of nitrogen oxides (NOx) using NH3 as a reductant agent in the presence of excess oxygen. These catalysts were characterized by FTIR, XRD, SEM-EDS, and H2-TPR meth...

In this study, an effective low-temperature method was developed, for the first time, for the synthesis of bismuth titanate nanobelts by using Na2Ti3O7 nanobelts as the reactants and templates. The experimental procedure was based on ion substitution followed by a nanoscale solid-state reaction. In the first step, Na2Ti3O7 nanobelts were soaked in a bismuth nitrate solution where ion substituti...

The current research was focused on synthesizing potassium sodium niobate (KNN) piezoelectric ceramics for the system (K0.48Na0.52) NbO3   by high energy ball milling process for 15h at the speed of 300 rpm.  The blended nano-crystalline powder was calcined in conventional box furnace at 700oC, 800oC and 900oC for duration of 5h, 7h and 10h.  Diffraction result of calcine powder confirmed the f...

Novel reusable magnetic carbon microspheres (MCMs) were prepared by hydrothermal method with glucose as carbon source and Fe3O4 nanoparticles as magnetic raw materials. And adsorption performance of MCMs for sulfonamide removal from water was investigated in detail. The results indicated that the calcination temperature and calcination time had significant effects on the surface area and its vo...

A simple and inexpensive electrospinning technique was used to synthesize 8 mol% yttria-stabilized zirconia (8YSZ) ceramic nanofibers having average diameter of ~200 nm after calcination. As-spun nanofibers after subjected to pre-selected time-temperature calcination profile retained excellent fiber morphology and were phase transformed, enhancing its further applicability in medical field. The...

Limestone calcination reaction seems to be a very simple and straight-forward reaction. However, there are numerous critical variables that exert profound effect on lime burning operations. The factors and variables that affect the burning of limestones must be considered in the selection, design and optimization of the calcininig equipment. Limestone burning in a vertical kiln often presents c...

The effects of chemical composition and preparation conditions, especially calcination atmosphere, water content and oxygen content on the catalytic performances of MoVTeNbO mixed oxide catalyst system for the selective oxidation of propane to acrylic acid have been investigated and discussed. Among the catalysts studied, the Mo1.0V0.3Te0.23Nb0.12O catalyst calcined in inert atmosphere under a ...

A range of catalysts comprising of platinum supported on silica, prepared by an impregnation method, have been studied for the total oxidation of naphthalene, which is a representative Polycyclic Aromatic Hydrocarbon. The influence of platinum loading and calcination temperature on oxidation activity was evaluated. Increasing the platinum loading up to 2.5 wt.% increased the catalyst activity, ...

Hydroxide-metal sludges from electroplating industry are a potential source of environmental contamination due to their high content of heavy metals. The incorporation of these residues in a ceramic matrix can be a promising way to suppress the harmful effect of metals normally present in those sludges. This work reports the role of the mixing time between the waste and ceramic materials and of...

Necklace-like MgO/TiO2 heterojunction structures were synthesized by a simple and economical precursor calcination method for the first time. The obtained unique MgO/TiO2 heterojunction structures exhibit an excellent removal performance towards toxic As(v) ions combined with good photocatalytic properties towards organic dyes.