نتایج جستجو برای: طرح xrd

تعداد نتایج: 104017  

Journal: :Journal of the American Chemical Society 2005
Darren H Brouwer Richard J Darton Russell E Morris Malcolm H Levitt

Since zeolites are notoriously difficult to prepare as large single crystals, structure determination usually relies on powder X-ray diffraction (XRD). However, structure solution (i.e., deriving an initial structural model) directly from powder XRD data is often very difficult due to the diffraction phase problem and the high degree of overlap between the individual reflections, particularly f...

Journal: :Acta Crystallographica Section A Foundations of Crystallography 2011

Journal: :Acta Crystallographica Section A Foundations of Crystallography 2005

Journal: :Journal of Polytechnic 2019

Journal: :Acta Crystallographica Section A Foundations of Crystallography 2011

Journal: :Acta Crystallographica 2021

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2008
Masafumi Suda Kozo Takayama Makoto Otsuka

Data from X-ray powder diffraction (XRD) were subjected to a partial least-squares regression analysis (PLS) to build a calibration model for predicting the polymorphic content of carbamazepine (CBZ). The effectiveness of the PLS method in the construction of calibration models was analyzed by a scientific approach based on a regulation vector. CBZ forms I and III were characterized by differen...

2018
Stina Holmgren Rondahl Fabien Pointurier Linnea Ahlinder Henrik Ramebäck Olivier Marie Brice Ravat François Delaunay Emma Young Ned Blagojevic James R. Hester Gordon Thorogood Aubrey N. Nelwamondo Tshepo P. Ntsoane Sarah K. Roberts Kiel S. Holliday

This work presents the results for identification of chemical phases obtained by several laboratories as a part of an international nuclear forensic round-robin exercise. In this work powder X-ray diffraction (p-XRD) is regarded as the reference technique. Neutron diffraction produced a superior high-angle diffraction pattern relative to p-XRD. Requiring only small amounts of sample, µ-Raman sp...

2015
Hoan Ho David E. Laughlin Jian-Gang Zhu

A technique based on x-ray diffraction (XRD) is introduced to understand the variation of the grain-to-grain ordering in FePt recording media. We classify the possible ways that the grains may be ordered into three types: homogeneous ordering, inhomogeneous ordering, and bipolar ordering. We study the possible impact of each type of ordering on the XRD spectra in terms of the relative angular p...

2009
Kheamrutai Thamaphat Pichet Limsuwan

In this study, the commercial TiO2 nanopowder and micropowder of anatase phase and rutile phase have been characterized by x-ray diffraction (XRD) and transmission electron microscopy (TEM). XRD patterns of nano-TiO2 in rutile and anatase phases exhibit broad peaks whereas both phases of micro-TiO2 demonstrate very sharp peaks. TEM images show that the grain size of TiO2 micropowders and TiO2 n...

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