Herein, we report that octahedral and spherical Cu2O samples with hollow structures are synthesized in high yield by reducing Cu(EDA)22+ complex with hydrazine. A series of experiments are carried out to investigate the factors which impact on the morphology of the Cu2O samples. It is observed that ethylenediamine (EDA) serves as a molecular template in the formation of hollow structure. Octahe...

Solid-phase spectrophotometry has been improved for the determination of the total and dissolved phosphate in water. The target phosphate-P at sub-µg dm(-3) to µg dm(-3) levels in a 20-cm(3) water sample was concentrated as the molybdenum blue species to 0.06 or 0.12 cm(3) using a Sephadex G-25 within 30 min, and gel beads were introduced to a 1.5-mm or 3-mm diameter flow cell having a 10-mm li...

Biological synthesis of nanoparticles is a relatively new emerging field of nanotechnology which has economic and eco-friendly benefits over chemical and physical processes of synthesis. In the present work, for the first time, the brown marine algae Sargassum muticum (S. muticum) aqueous extract was used as a reducing agent for the synthesis of nanostructure silver particles (Ag-NPs). Structur...

Where T is transmittance, I0 is intensity of incident light, I is intensity of transmitted light and Is is intensity of stray light. Stray light has an increasing influence on spectroscopic measurements at low levels of intensity, that is, high absorbances. The result is that stray light causes a negative bias in instrument response and eventually becomes the limiting factor for absorbance and ...

The MANTRA (Middle Atmosphere Nitrogen TRend Assessment) 2004 campaign took place in Vanscoy, Saskatchewan, Canada (52 N, 107 W) from 3 August to 15 September, 2004. In support of the main balloon launch, a suite of five zenith-sky and direct-Sun-viewing UV-visible ground-based spectrometers was deployed, primarily measuring ozone and NO2 total columns. Three Fourier transform spectrometers (FT...

We have developed automated methods for the trityl-on purification and quantification of synthetic oligonucleotides. Oligonucleotide purification is by solid-phase extraction cartridges using Amberchrom CG-50 resin on an XYZ-axis robotic system. Quantification is by OD260nm using an online UV-visible spectrophotometer with sipper. The purification of 20 oligonucleotides requires 5 min of user s...

In the present work, the ZnFe2O4 nanoparticle has been successfully synthesized. The obtained sample was characterized by X-ray diffraction (XRD), emission scanning electron microscopy (FE-SEM) and its optical property was examined by UV-Vis spectrophotometer. FE-SEM revealed that the particle size of the ZnFe2O4 of about 47 nm was synthesized. The photocatalytic performance under UV-Vis and vi...

A systematic study of the attenuation electromagnetic radiation in Nuclear Track Detectors (NTDs) is carried out. The gamma-ray, X-ray, UV, visible, and infrared NTDs are investigated using NaI(Tl) detector, Gas Electron Multiplier (GEM) UV-Vis spectrophotometer, FTIR spectrophotometer respectively. values some important parameters (e.g., optical depth, coefficient, etc.) three commercially ava...