By means of ultrasonication two fractions of the carboxymethylated chitin–glucan complex isolated from the cell walls of 13 the filamentous fungus Aspergillus niger were obtained. Elemental analysis as well as C NMR investigation of the high-molecular weight (M 680 kDa) and low-molecular weight (M 75 kDa) fractions revealed their essentially different w w chitin content. HPLC analysis of the fr...

A straightforward on-line monitoring of organic reactions by ultrasonication-assisted spray ionization mass spectrometry (UASI MS) is demonstrated in this work.

An investigation on viscosity was conducted 2 weeks after the Al2O3-water nanofluids having dispersants were prepared at the volume concentration of 1-5%. The shear stress was observed with a non-Newtonian behavior. On further ultrasonic agitation treatment, the nanofluids resumed as a Newtonian fluids. The relative viscosity increases as the volume concentrations increases. At 5% volume concen...

Under ultrasonication, the production of high quality graphene layers by exfoliation of graphite was achieved via addition of tiopronin as an antioxidant.

BACKGROUND Generation-3 (Gen-3) biosensors and advanced enzyme biofuel cells will benefit from direct electron transfer to oxidoreductases facilitated by single-walled carbon nanotubes (SWNTs). METHODS Supramolecular conjugates of SWNT-glucose oxidase (GOx-SWNT) were produced via ultrasonic processing. Using a Plackett-Burman experimental design to investigate the process of tip ultrasonicati...

In high-throughput ultrasonication enhanced hollow-fiber liquid-phase microextraction (H-U-HF-LPME), ultrasonication was introduced into HF-LPME to enhance the mass transfer rate of the analytes in the two immiscible liquid phases, which resulted in a very short time for extraction equilibrium and a high-throughput analysis. Several parameters were investigated and optimized (such as extraction...

OBJECTIVES The potential applications and industrial production of multi-wall carbon nanotubes (MWCNT) have raised serious concerns about their safety for human health and the environment. The present study was designed to examine the in vitro cytotoxicity and genotoxicity of MWCNT and UICC chrysotile A (chrysotile). METHODS Cytotoxicity using both colony formation and lactate dehydrogenase (...

This study focuses on the extraction of nanocrystalline cellulose ( NCC) from the dried stalk of Corchorus olitorius, commonly known as jute, using a combination of a microwave-assisted alkaline peroxide pulping process (AHP) and ultrasonication. Dried jute stalk powder was pretreated using sodium hydroxide under microwave irradiation for the removal of lignin. The partially delignified sample ...