the magnetite (fe3o4) – agar nanocomposite was prepared by co-precipitation of fe (iii) and fe (ii) ions for the first time. the obtained samples were characterized by x-ray diffraction, fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. ft-ir results confirm the formation of fe3o4 nanoparticles in agar matrix. the xrd results revealed th...

this paper reports the synthesis of polypyrrole coated sno2/znoelectrospunnanofibers via vapor phase polymerization method. in order to prepare one dimensional (sno2-zno)/polypyrrole with the core sheath structure, first sno2-zno composite nanofibers were synthesized via electrospinning method followed by adsorption of fe3+ on the surface of the sno2-zno nanofibers and finally pyrrole was polym...

the purpose of the current research is investigating the phenylalanine removal by using magnetic nanoparticles (fe3o4) from water samples. the effect of ph, contact time and phenylalanine concentration on phenylalanine adsorption efficiency by magnetite nanoparticles are studied in a batch system. transmission electron microscopy (tem), x-ray diffraction patterns (xrd) and fourier transform inf...

The crystal phase of Au-NWs is assessed by means of high-resolution transmission electron microscopy (HR-TEM). NWs are dispersed on a transmission electron microscopy (TEM) grid and imaged with a JEOL 4000EX-II TEM. Figure S-2(a) shows a HR-TEM lattice imaging of a representative Au-NW. The measured interplanar spacing (3.74 Å) is consistent with the (110) planes of a CdSe crystal with the wurt...

Actinide materials demonstrate a wide variety of interesting physical properties in both bulk and nanoscale form. To better understand these materials, a broad array of microscopy techniques have been employed, including transmission electron microscopy (TEM), electron energy-loss spectroscopy (EELS), energy dispersive X-ray spectroscopy (EDXS), high-angle annular dark-field imaging (HAADF), sc...

in this paper, nickel oxide (nio) nanoparticles have been prepared by solid state thermal decomposition of an acyclic nickel(ii) complex (1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(ii) chloride, [nil]cl2, in an electrical furnace at optimal temperature, 450 ºc for 3.5 h. the nickel(ii) complex is obtained via solid state synthesis using nickel(ii) chloride and tetradentate o4 acyclic ligan...

manganese oxide nanoparticles (mn3o4-nps) were prepared using precipitation method. the prepared nanoparticles were characterized by a number of techniques, including x-ray diffraction (xrd) analysis, scanning electron microscopy (sem), transmission electron microscopy (tem) and fourier transforms infra red (ft-ir) spectroscopy. the xrd pattern showed that the structure of mn3o4-nps was tetrago...

in  this  work,  a  new  hybrid  organometallic-inorganic  hybrid nanomaterial was prepared by immobilization of acetyl ferrocene on the  surface  of magnetite  nanoparticles. covalent  grafting of silica coated magnetite nanoparticles (scmnps) with 3-aminopropyl triethoxysilane gave aminopropyl-modified magnetite nanoparticles (ampscmnps). then, schiff base condensation  of ampscmnps with acet...

V2O5/SiO2 nanoparticles was prepared via an one-pot sol gel method from vanadyl- acetylacetonate and tetraethylorthosilicate in refluxing MeOH, followed by calcination at 700 °C for 2 hours. The resultant nanoparticles was characterized by means of scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), TGA and FTIR techniques. Rapid and efficient ar...

Silica  coated magnetite  nanoparticles were  covalent  grafted with  3-aminopropyl trimethoxysilane  to give APTSCMNPs. Reaction of  the resulted nanomaterial with 4-formyl benzo-12-crown-4 ether afforded FB12C4/APTSMNPs  nanocomposite  material  in  which  the  crown ether  moiety  was  attached  through  propyl  chain  spacer. Characterization of  the prepared nanocomposite was performed wit...