in this study, 60 composite samples of dill and onion from two different cultivated areas in khozestan province, iran, were collected and analyzed for the presence and determination of lead and cadmium by flame atomic absorption spectrometry. samples were burned according to aoac at 450 °c, and the residue was dissolved in nitric acid. lead and cadmium contents were determined using calibration...

new advances in mass spectrometry-based proteomics technology are having amajor impact on our understanding of how human spermatozoa acquire their capacity for fertilization. a complete analysis of the proteins found in the human spermatozoa is essential for understanding the events leading up to, and including, fertilization and early embryo development. in this short review, we have collected...

in this study, a rapid, simple and sensitive ion mobility spectrometry (ims) method with corona discharge as ionization source was described for the morphine determination in human urine. morphine was extracted and purified from urine samples using solid phase extraction procedure with c18 column. it can offer the clean extracts which no extra peaks were observed in ims. under operating experim...

a new method for the determination of trace copper(ii) in food samples by cloud point extraction(cpe) combined with flame atomic absorption spectrometry(faas) is presented and evaluated. the method is based on the fact that hydrophobic complex of copper(ii) with sodium diethyldithiocarbamate (ddtc) was formed at ph 6.0 and subsequently the hydrophobic complex was extracted into surfactant-rich ...

reactions of free radicals and reactive oxygen species (ros) with biological molecules in vivo play an important physiological role in many diseases. 2,2-diphenyl-1-picrylhydrazyl (dpph) is a stable free radical and often used as a routine reagent to evaluate the antioxidant capacity of an antioxidant. this study was undertaken to investigate the free radical-scavenging and antioxidant activiti...

a new method for analysis of trace amount of rh(iii) ions by magnetic activated carbon modified with 2,3,5,6-tetra(2-pyridyl)pyrazine (mac/tppz) as the magnetic sorbent has been proposed. the proposed adsorbent was found to be advantageous over conventional solid phase extraction (spe) in terms of operational simplicity and low time-consuming. the experimental parameters affecting the extractio...