Spark Plasma Sintering (SPS) is used to fabricate Titanium-Niobium-Zirconium-Tantalum alloy (TNZT) powder-based bioimplant components with controllable porosity. The developed densification maps show the effects of final SPS temperature, pressure, holding time, and initial particle size on final sample relative density. Correlations between the final sample density and mechanical properties of ...

Using the spark plasma sintering (SPS) method, hydroxyapatite (HAp) material was densified using a hydroxyapatite powder (RND Korea, 45 μm, purity 98 +%). The HAp was nearly completely dense with a relative density of up to 97 % after the simultaneous application of 60 MPa of pressure and about 30 minutes of electric current without significant change in the grain size. The average grain size o...

In the present work, nanoceramics of Li5La3Ta2O12 (LLT) lithium ion conductors with the garnet-like structure are fabricated by spark plasma sintering (SPS) technique at different temperatures of 850°C, 875°C, and 900°C (SPS-850, SPS-875, and SPS-900). The grain size of the SPS nanoceramics is in the 50 to 100 nm range, indicating minimal grain growth during the SPS experiments. The ionic condu...

ransparent polycrystalline alumina (PCA) is a promising replacement for sapphire. Its optical properties however are highly dependent on the rain size and residual porosity which need to be controlled for real inline transmittances (RIT), that are high enough for possible applications. To achieve high RITs, doping as well as pressure assisted sintering is often used. In this study spark plasma ...

The development of new carbon nanofibers-ceramic nanocomposite materials with excellent mechanical, thermal and electrical properties is interesting for a wide range of industrial applications. Among the ceramic materials, zirconia stands out for their excellent mechanical properties. The main limitations in the preparation of this kind of nanocomposites are related with the difficulty in obtai...

Pure magnesium (Mg) powders with stearic acid added as process control agent (PCA) were mechanically milled (MMed) using a vibration ball mill. The MMed consolidated into bulk materials by the spark plasma sintering (SPS). Changes in hardness, thickness and solid-state reactions of SPS have been examined hardness measurements, vernier caliper an X-ray diffraction (XRD), respectively. Vickers ma...

The synthesis of AlN and TiB2 by spark plasma sintering (SPS) and the effect of Nb2O5, Y2O3 and ZrO2 additions on the mechanical properties and densification of the produced composites is reported and discussed. After the SPS process, dense AlN and TiB2 composites with Nb2O5, Y2O3 and ZrO2 were successfully prepared. X-ray diffraction analysis showed that in the AlN composites, the addition of ...

10 Abstract CexZr1-xO2 (x = 0.10, 0.16 and 0.33) nano11 crystalline powders were obtained by a two-step synthesis 12 technique and sintered by spark plasma sintering (SPS). As 13 consequence of the reduction of Ce to Ce species by 14 carbon in the graphite environment in SPS, phase assem15 blies including tetragonal, monoclinic and pyrochlore 16 phases were generated in the ceramics during the ...