نتایج جستجو برای: single crystal x
تعداد نتایج: 1554422 فیلتر نتایج به سال:
The co-crystal compound of 4,4'-bipyridine 3-nithrophthalic acid (1) was obtained by the reaction of 4,4'-bipyridine, 3-nithrophthalic acid and calcium chloride (1:1:1 molar ratio) in solvents mixture H2O/MeOH under solution condition. The crystal structure of this compound was determined by elemental analysis, IR spectroscopy and single crystal X-ray diffraction method. Crystallographic data f...
9-aminoacridinum acridine-9-carboxylate (1) as a proton transfer ion pair was obtained by the reaction of 9-aminoacridine, acridine-9-carboxylic acid and zinc nitrate (1:1:1 molar ratio) in solvents mixture H2O/MeOH under reflux condition. The crystal structure of this compound was determined by elemental analysis, IR spectroscopy and single crystal X-ray diffraction method. Crystallographic da...
The new complex of [H2en][Cu(pydc)2].2H2O (1) (where H2en and pydc are ethylenediammonium and 2,6-pyridinedicarboxylate, respectively) was synthesized by the reaction of a mixture of ethylenediamine (en) and 2,6-pyridinedicarboxylic acid (H2pydc) in a mixture of CH3OH/H2O as solvent. This complex was fully characterized by elemental analysis, IR, UV–Vis spectroscopy as well as single-crystal X-...
Single crystals of CdTe were grown by the sublimation and condensation technique in a silica, under an argon gas now, and also by alloing cadmium tcJloride transport within an evacuated silica ampoule. X-ray powder diffraction patlerns prepared from each group of grown crys tals showed the crystal structure of the examined samples to be zinc-blend race-cent red cubic. Transmission electr...
Hydrothermal synthetic were studied for the preparation of coordination polymeric material basedon Ag (I) and 4, 4"-bipy. A polymeric compound [Ag (4, 4'-bipy)].NO3. (I), was prepared andstructurally characterized by single crystal X-ray diffraction. Compound 1(91% yield) was isolatedfrom the reaction of AgNO3 with 4, 41bipy in 2:1 molar ratio. In compound I. each silver (I) islinked to two nit...
Cd0.96Zn0.04Te crystals were grown using vapor phase gas transport method (VPGT). The results show that dendritic crystals with grain size up to 3.5 mm can be grown with this technique. X-ray diffraction and Laue back-reflection patterns show that dendritic crystals are single-phase, whose single crystal grains are randomly oriented with respect to the gas-transport axis. Electrical measureme...
The synthesis and single-crystal X-ray structure determination of the title compound (phen)Pb(02CMe) is described. The complex crystallizes in the monoclinic space group P2 /c, a = 7.823(3), b = 12.421(4), c = 9.262(2) ?, ? = 79.92(3)", Z = 4, yielding R 0.048 for 3210 independent reflections. The coordination number around the lead atom is six. [Pb-N 2.54(2), 2.56(4)],[Pb-0, 2.19-2.22]
Abstract: fabricated. Modifications carried out in different parts of the old system in order to control mostof the growth parameters with more accuracy. The fabricated system was used to grow sapphiresingle crystals with almost 10 mm in diameter and 50 mm in length. The crystallinity andstructure of the grown crystals were characterized by computer aided single crystal X-raydiffraction techniq...
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