نتایج جستجو برای: ray diffraction measurement then
تعداد نتایج: 1484604 فیلتر نتایج به سال:
The measurement of X-ray diffraction data from macromolecular crystals for the purpose of structure determination is the convergence of two processes: the preparation of diffraction-quality crystal samples on the one hand and the construction and optimization of an X-ray beamline and end station on the other. Like sample preparation, a macromolecular crystallography beamline is geared to obtain...
in the current paper,nanostructured nickel oxide (nio) were synthesized by co-precipitation method using nickel(ii) chloride hexahydrate (nicl2.6h2o) and sodium hydroxide (naoh) as starting material. structural, optical and magnetic properties of nanostructures were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), atomic force microscope (afm), uv–vis absorption; fo...
In this research, CdS nanoparticles and core/shell CdS/ZnS nanoparticles were prepared by using aqueous solution method and used 3-mercaptopropionic acid (MPA) as capping molecule. The effect of ZnS shell on optical and structural properties of CdS was investigated. X ray diffraction patterns of CdS nanoparticles at the room temperature and after heat treatment show zinc blende structure. X ray...
We describe the application of synchrotron X-ray diffraction and neutron micro-tomography to three ancient bronze coins from the Mediterranean coast of Israel. Key questions are whether neutron tomography can contribute to the reading of features on corroded coins by allowing the corrosion crust to be stripped away in cyber-space using surface and volume rendering techniques, and to what extent...
introduction individual x-ray diffraction patterns of biological tissues are obtained via interference of coherent scattering with their electrons. many scientists have distinguished normal and cancerous breast tissue, bone density, and urinary stone types using the x-ray diffraction patterns resulting from coherent scattering. the goal of this study was to introduce an optimized method for obt...
The focus in macromolecular crystallography is moving towards even more challenging target proteins that often crystallize on much smaller scales and are frequently mounted in opaque or highly refractive materials. It is therefore essential that X-ray beamline technology develops in parallel to accommodate such difficult samples. In this paper, the use of X-ray microradiography and microtomogra...
this work has setup to determine the effects of a solvent on the structure and properties of polypropylene fibres with different physical structures. samples of continuous filament yarns with different physical structures (partially oriented (poy) and drawn yarns) are treated with decahydronaphthalene (decalin) at 28, 55, 75 and 95oc. at 95oc, the samples are dissolved completely in decalin and...
The formation of two-dimensional halogen-bonded layers of 4,4'-bipyridyl and 1,4-diiodotetrafluorobenzene was observed on a graphite surface at sub-monolayer coverage using synchrotron X-ray diffraction; the use of the diffraction technique enabled, for the first time, the measurement of I···N halogen bonding distances in a two-dimensional cocrystal and the identification of the halogen bonding...
In this work, Ce-YIG nanoparticles with nominal composition of Y3-xCexFe5O12 (x = 0, 0.1, 0.3, 0.4, 0.5, 0.6, 0.7 and 0.8) were first fabricated by sol-gel method and then the influence of the cerium substitution on the structural and magnetic properties of garnet nanoparticles were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), fourier transform infrared (FT-IR)...
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