In the present paper, we have synthesized the NiO nanoparticles with chemical route. Further, the uniform suspensions of NiO nanoparticles in ethylene glycol of different concentrations have been prepared. Samples were characterized with Acoustical Particle Sizer (APS-100) for the frequency dependent ultrasonic attenuation in the respective samples; subsequently the particle size determination ...

Photoelectrochemical hydrogen evolution is a promising avenue to store the energy of sunlight in the form of chemical bonds. The recent rapid development of new synthetic approaches enables the nanoscale engineering of semiconductor photoelectrodes, thus tailoring their physicochemical properties toward efficient H2 formation. In this work, we carried out the parallel optimization of the morpho...

A unique hexagonal sheet-shaped NiO/CoO/Fe2O3 composite with irregularly shaped nanoparticles was fabricated for the first time through a simple co-precipitation and hydrothermal method. The NiO/CoO/Fe2O3 composite was characterized by numerous techniques (TEM, HRTEM, PXRD, EDX, ICP-AES, BET, and XPS) to confirm its structure and composition. This structure of the NiO/CoO/Fe2O3 composite may en...

In this paper, nickel oxide (NiO) nanoparticles have been prepared by solid state thermal decomposition of an acyclic nickel(II) complex (1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II) chloride, [NiL]Cl2, in an electrical furnace at optimal temperature, 450 ºC for 3.5 h. The nickel(II) complex is obtained via solid state synthesis using nickel(II) chloride and tetradentate O4 acyclic ligan...

Transitional metal oxide nanoparticles as advanced environment and energy materials require very well absorption performance to apply in practice. Although most metal oxides are based on crystalline, high activities can also be achieved with amorphous phases. Here, we reported the adsorption behavior and mechanism of methyl blue (MB) on the amorphous transitional metal oxide (Fe, Co and Ni oxid...

Self-organized TiO 2 nanotubes (TNTs) with average inner diameter of 109 nm, wall thickness of 15 nm, and tube length of 7– 10 μm were loaded with nickel oxide (NiO) nanoparticles via incipient wet impregnation method. The molar concentration of Ni(NO 3 ) 2 ⋅6H 2 O aqueous solution varied in a range of 0.5M–2.5M. The samples were characterized for crystalline phase, morphology, topography, chem...

The electronic structure of NiO nanometric planar islands on highly oriented pyrolitic graphite has been studied by means of the Ni 2p and O 1s x-ray absorption spectra. The O 1s spectrum of the early stages of growth shows a double peak at threshold which is attributed to a splitting of the unoccupied Ni eg states. This spectrum is compared to previous results for 3 nm NiO nanoparticles which ...

The effect of NiO nanoparticles on the rheological and volumetric properties of dilute solutions of starch-NaOH-H2O, PEG400-PEG2000 and PEG400-PEG6000 were investigated. Achieve this aim requires to prepare the stable nanofluids. Therefore, nanoparticles of NiO were added to these solutions and dispersed by a shaker and an ultrasonic bath for making the homogeneous nanofluids. The UV-Vis spectr...

the combination of graphene (gr) and nickel oxide nanoparticles (nio nps) yields nanostructured electrochemical sensor formed a novel kind of structurally uniform and electrocatalytic activity material. in cyclic voltammetry (cv) studies, in the presence of ep, nio/gr composite modified electrode shows a significantly higher current response for ep oxidation. based on differential pulse voltamm...

NiO-nanoflakes (NiO-NFs) grafted Ni-nanorod (Ni-NR) arrays stuck out of the porous anodic aluminum oxide (AAO) template are achieved by a combinatorial process of AAO-confined electrodeposition of Ni-NRs, selectively etching part of the AAO template to expose the Ni-NRs, wet-etching the exposed Ni-NRs in ammonia to obtain Ni(OH)2-NFs grafted onto the cone-shaped Ni-NRs, and annealing to transfo...