The laboratory for instrumental neutron activation analysis at the Reactor Institute Delft, Delft University of Technology uses a network of 3 gamma-ray spectrometers with well-type detectors and 2 gamma-ray spectrometers with coaxial detectors, all equipped with modern sample changers, as well as 2 spectrometers with coaxial detectors at the two fast rabbit systems. A wide variety of samples i...

Instrumental neutron activation analysis (INAA) was applied for the accurate and precise determination of minor and trace elements in small-sized aliquants (1 to 2 mg) of two certified reference materials (CRM), NIES No. 8 and NIST 1632c. Four laboratories used either comparative- or k0-INAA, or both, and repeated the analysis more than ten times for each CRM. Based on z-scores and zeta scores ...

Introduction Neutron activation analysis (NAA) is a nuclear process used for determining the concentrations of elements in a vast amount of materials. NAA relies on excitation by neutrons so that the treated sample emits gamma-rays. It allows the precise identification and quantification of the elements, above all of the trace elements in the sample. NAA has applications in chemistry but also i...

An analysis of neutron diffraction data of liquid deuterated terr-butanol at room temperature to determine its molecular conformation is presented. Being a big molecule of 15 sites, the analysis is tricky and needs careful consideration. The resulting molecular parameters are compared with those obtained from other experimental data analysis and model calculations. The information about the int...

As a continuation of diffraction work on melts from eutectic binary systems such as Al-Sn [1], Au-Co [2], and Bi-Cu [3] an investigation of melts from the eutectic system Sn-Zn by means of neutron diffraction will be described in the present work. The liquidus lines in the constitution diagrams of these systems always show a point of inflection, so th a t segregation tendency in molten state is...

The structures of both known forms of the polymorphic material ortho-acetamidobenzamide, C(9)H(10)N(2)O(2), have been determined by low-temperature neutron single-crystal diffraction. Neutron diffraction allows the full description of the H-atom positions in this molecular material, which is vital in benchmarking related crystal-structure predictions. Significant conformational differences are ...

The crystal structure of the high temperature phase of anilinium bromide, CeH5NH3®Br , was studied by X-ray and neutron diffraction at T = 343 K . The refinement supports disordered positions of the —NH3® group. A split-atom model is proposed which includes disorder of the benzene ring. The thermal parameters, hydrogen bond distances, and other experimental data (NMR, N Q R , inelastic neutron ...