The effect of different processing routes on the microstructure of nanocrystalline ceria powder has been investigated. The nanocrystalline ceria is produced by solid state high energy ball milling (HEBM) and liquid state solution combustion synthesis (SCS) method. The liquid state route consists of a high temperature combustion reaction to form ceria from an aqueous solution of cerium ammonium ...

PURPOSE The purpose of the present study was to evaluate the flexural strength of the joint between glass-infiltrated alumina frames and the experimental adjusting agent (MA modifier) that contains alumina and magnesia. METHODS A commercially available adjusting agent (Optimizer), a slurry of alumina powder (Alumina modifier), and a bulk specimen (joint-free alumina) were used as controls. Be...

This Standard Reference Material (SRM) consists of a sintered alumina disc intended for use in calibration of X-ray powder diffraction equipment with respect to line position and intensity as a function of 2 angle. The solid form of the SRM eliminates any variability in intensity measurements introduced by the sample loading procedure. A unit of SRM 1976b consists of a sintered alumina disc ap...

Al2O3:SiOC nanocomposites were synthesized by thermal treatment of fumed alumina nanoparticles modified by phenyltrimethoxysilane. The effect of annealing temperature in inert ambient on structure and photoluminescence of modified alumina powder was studied by IR spectroscopy as well as photoluminescence spectroscopy with ultraviolet and X-ray excitation. It is demonstrated that increase of ann...

9 = 0.6 I / s ' 7 = 6.0 0 7 = 2 4 i ti 3 = 6 0 Through close control over green-state powder processing, pure alumina ceramics of 0.5-pm grain size were obtained by sintering at 1250°C. The static grain growth of this material was modest at temperatures below 1300°C. However, dynamic grain growth occurred rapidly during superplastic deformation. Therefore, although the ultrafine-grained alumina...

The quality of the refractories applied on integrated gasification combined cycle should be a key factor that affects both the reliability and the economics of gasifier operation. To enhance the workability of chromia/alumina castables, three types of ultrafine alumina powder were added to improve the workability. Densification behavior of such castables in the presence of ultrafine alumina was...

This paper reports a study on nanocrystalline ceria powder prepared by high energy ball-milling and combustion synthesis methods. The combustion synthesis was carried out using ceric ammonium nitrate as oxidizer and citric acid, glycine or citric acid plus glycine as fuel. The minimum crystallite size of ceria powder is obtained by combustion synthesis of ceric ammonium nitrate and citric acid....

Nanocrystalline nickel manganite (NiMn2O4) powder with a pure cubic spinel phase structure was synthesized via sol-gel combustion and characterized XRD, FT-IR, XPS SEM. The mixed sodium alginate gel to form nano-biocomposite gel, dried at room temperature thick film FT-IR DC resistance AC impedance of sensor test structures obtained by drop casting the onto interdigitated PdAg electrodes on an ...

Aluminum/alumina composites are used in automotive and aerospace industries due to their low density and good mechanical strength. In this research, the effect of mechanical stirring of slurry in liquid-solid phase temperature and injection of alumina powder with inert gas (Ar) on microstructure and mechanical properties of Al-A356 alloy is investigated. In order to improve of the wettability a...