A novel Congo red (CR) derivatized silica stationary phase was prepared and packed into a fused silica capillary tube for nano-flow HPLC. A variety of analytes including poly-aromatic hydrocarbons, parabens, acids, sulfonamides, bases, and nucleosides were successfully separated using the CR. In comparison with commercial ODS columns, this new stationary phase has a different separation mechani...

Analysis of phosphotyrosine and phosphoserine containing peptides by nano-electrospray Fourier transform ion cyclotron resonance (FTICR) mass spectrometry established electron capture dissociation (ECD) as a viable method for phosphopeptide sequencing. In general, ECD spectra of synthetic and native phosphopeptides appeared less complex than conventional collision activated dissociation (CAD) m...

The reaction of levulinic acid production from glucose has a stage that requires high temperature and activation energy so in this catalyst is needed. required must have lewis site bronsted the acidity very influential for successful levulonic acid. Silica nickel phosphate catalysts sites Ni metal phosphoric silica groups. was measured using pyridine ammonia adsorption method center strength TG...

The nano-sized silica fillers reinforced poly(ether ether ketone) (PEEK) composites were fabricated by means of compression molding technique. he nano-sized silica, measuring 30 nm in size, was firstly modified by surface pretreatment with stearic acid. The performances and properties f the resulting PEEK/SiO2 nanocomposites were examined in terms of tensile loading, hardness, dynamic mechanica...

This study is focused on synthesis of nano-colloidal silica via alkaline water glass solution. Sodium ions of water glass were removed by cation exchanging in a resin column to obtain the silicic acid which was titrated to the solution of sodium silicate. Concentration of the colloidal silica and pH value of the solutions were controlled using different concentrations of alkaline sodium silicat...

background: the aim of this study was to compare the effects of conventional acid etching and laser etching on the nano-mechanical properties of the dental enamel using nano-indentation test. materials and methods: in this experimental in vitro study, buccal surfaces of 10 premolars were divided into three regions. one of the regions was etched with 37% phosphoric acid and another etched with e...