Mechanically Activated Self-propagating High temperature Synthesis (MASHS) is the method which is used to promote self-propagating synthesis by increasing activity of reactants and increase the purity of products. In this study Ti 2 AlC and Ti3AlC2 max phases were synthesized by using mechanically activated self-propagating high temperature synthesis (MASHS) and samples reactivity and phase str...

A rapid and efficient method for the synthesis of bis-thiazolidinones has been achieved by pseudo five-component reaction of aldehydes, ethylenediamine and thioglycolic acid in the presence of nano-NiZr4(PO4)6 as catalyst under microwave irradiation. Nano-NiZr4(PO4)6 has been characterized by powder X-ray diffraction, scanning electronic microscopy (SEM), energy dispersive spectroscopy (EDS), v...

Present work describes the synthesis of coumarin Mannich bases 4-7 by the application of Mannich reaction on 7-hydroxy-4-methyl coumarin 3 using conventional as well as microwave technology to compare the feasibility, reaction time and yield of the product. For this, 7-hydroxy-4-methyl coumarin 3 was prepared using Pechmann condensation reaction and Mannich bases (4-7) were synthesized by the r...

Application of a dynamic microwave power system in the chemical synthesis of some phenothiazine and quinoline derivatives is described. Heterocyclic ring formation, aromatic nucleophilic substitution and heterocyclic aldehydes/ketones condensation reactions were performed on solid support, or under solvent free reaction conditions. The microwave-assisted Duff formylation of phenothiazine was ac...

silver nanoparticles (nps) have been the subjects of researchers because of their unique properties ( e.g., size and shape depending optical, antimicrobial, and electrical properties). a variety of preparation techniques have been reported for the synthesis of silver nps; notable examples include, laser ablation, gamma irradiation, electron irradiation, chemical reduction, photochemical methods...

Microwave synthesis of two porous nickel glutarates was compared with conventional hydrothermal synthesis. The cubic nickel glutarate, [Ni20(C5H6O4)20(H2O)8] x 40 H2O (1), was synthesized by conventional electrical heating in several hours or days, depending on synthesis temperature. Crystallization was greatly accelerated by microwave irradiation, in which more stable, tetragonal nickel glutar...

a phosgene-free synthesis of symmetrical n,n'-disubstituted urea by the reaction of aromatic and aliphatic primary amines and urea promoted by  microwave irradiation in the presence of a suitable energy-transfer solvent such as n-n-dimethylacetamide is described.

The water core of reverse micelles has been extensively used as the site for synthesis of a variety of materials. However, water-in-oil reverse micelles have a limited range of temperatures over which they are stable as a single phase. Directing heat to the water cores, the usual site of synthesis without heating the bulk provides added opportunities for synthesis. Microwave radiation is a meth...

This paper mainly described the new instruments of microwave-promoted organic synthesis which were appraised, and several microwave-assisted synthetic reactions, such as esterification reaction, orthogonal experimental design and fentanyl synthetic reactions. In comparison with traditional methods of organic synthesis, microwave-assisted chemistry could make high-speed processing of chemical tr...

This paper focused on a simple approach for synthesis of molybdenum oxide (MoO3) nanoparticles and reports a facile route for synthesis of such nanoparticles, using microwave irradiation as a homogenous and powerful source of heating, using ethylene glycol as the solvent and heating medium. For more investigations, besides microwave heating, the obtained solutions were also treated by conventio...