نتایج جستجو برای: microwave assisted synthesis

تعداد نتایج: 576400  

2013
Ramesh G

Microwave assisted combustion synthesis is used for fast and controlled processing of advanced ceramics. Single phase and sinter active nano crystalline alpha alumina powders were successfully synthesized by different fuel-to-oxidant molar ratios using aluminium nitrate as an oxidiser, glycine as a reducing agents and millipore water as a solvent by microwave assisted combustion synthesis. Ther...

Journal: :Organic & biomolecular chemistry 2008
Lakshminath Sripada Jesse A Teske Alexander Deiters

A concise synthesis of phenanthridines via a microwave-assisted [2+2+2] cyclotrimerization reaction has been developed.

2012
Hasnah Osman Afsheen Arshad Chan Kit Lam Mark C Bagley

UNLABELLED BACKGROUND Coumarin derivatives exhibit a wide range of biological properties including promising antioxidant activity. Furthermore, microwave-assisted organic synthesis has delivered rapid routes to N- and O-containing heterocycles, including coumarins and thiazoles. Combining these features, the use of microwave-assisted processes will provide rapid access to a targeted coumarin...

Journal: :caspian journal of chemistry 2013
seyed naser azizi abdolrauf samadi-maybodi mohammad hossein fatemi neda asemi

perlite or pearl stone is a natural glass which has formed by rapid cooling of viscous lava or magma. perlite is mainly composed of silica, aluminum, potassium and sodium. in this experiment, perlite was used as a low-cost source of si and al to synthesis of sodalite zeolite using the alkaline hydrothermal treatment. a statistical taguchi design of experiments was employed to evaluate the effec...

Abdolrauf Samadi-Maybodi Mohammad Fatemi, Neda Asemi Seyed Azizi,

Perlite or pearl stone is a natural glass which has formed by rapid cooling of viscous lava or magma. Perlite is mainly composed of silica, aluminum, potassium and sodium. In this experiment, perlite was used as a low-cost source of Si and Al to synthesis of sodalite zeolite using the alkaline hydrothermal treatment. A statistical Taguchi design of experiments was employed to evaluate the effec...

Journal: :journal of nanostructures 0
meisam hasanpoor department of materials science, faculty of engineering, tarbiat modares university, tehran, iran houman fakhr nabavi department of materials science, faculty of engineering, tarbiat modares university, tehran, iran mahmood aliofkhazraei department of materials science, faculty of engineering, tarbiat modares university, tehran, iran

in present study we studied using green routes for microwave assisted synthesis of alumina nanoparticles from aluminum nitrate. it was revealed that when plant extracts are used, no specific stabilizer is needed. structural characterization of nanoparticles was studied using x-ray diffraction that showed semi-crystalline structure for two of plant extracts, other xrd patterns had no significant...

Journal: :international journal of nanoscience and nanotechnology 2013
p. boroojerdian

semiconductor nanoparticles exhibit size dependent properties due to quantum confinement effect that arenot present in their bulk counterparts. in this work, extremely fine and pure sno2 nanoparticles of ~1.1nm size were synthesized by a solution process, in which amorphous precipitate of sno2 was crystallizedby microwave heating. the particles sizes varied from ~1.1 to ~2.7 nm. by xrd analysis...

2013
Yashumati R. Bhardwaj Monika Chauhan Ashutosh Pareek Dharma Kishore

Present work describes the synthesis of coumarin Mannich bases 4-7 by the application of Mannich reaction on 7-hydroxy-4-methyl coumarin 3 using conventional as well as microwave technology to compare the feasibility, reaction time and yield of the product. For this, 7-hydroxy-4-methyl coumarin 3 was prepared using Pechmann condensation reaction and Mannich bases (4-7) were synthesized by the r...

2012
Jolly Jacob

Revolution in organic compound synthesis has been promoted by microwave assisted organic syntheses (MAOS) by which small molecules are built up into large polymers in a fraction of time. The need for different organic compound libraries for drug discovery, biomaterial development, automated library screening; proteomics etc has supported the emergence of innovative technologies for rapid combin...

Journal: :Chemical communications 2010
Herbert Waldmann Luc Eberhardt Kathrin Wittstein Kamal Kumar

A silver catalyzed and microwave assisted one-pot cascade synthesis provides efficient access to diverse alkaloid-inspired scaffold classes, and a concise and efficient total synthesis of homofascaplysin C and fascaplysin.

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