Beta lactam antibiotics are widely used in therapy of cattle, particularly for the treatment of mastitis.  Over 95% of residue testing in dairies in Bosnia and Herzegovina is for Beta lactams. The aim of this paper is to compare the efficacy of three most common screening tests for Beta lactam residues in cow's milk in our country. The tests used in the study are SNAP β Lactam test (Idexx), Ros...

The STAR protocol is a Five Plate Test (FPT) developed several years ago at the Community Reference Laboratory (CRL) for the screening of antimicrobial residues in milk and muscle. This paper presents the validation of this method according to European Decision 2002/657/EC and to an internal guideline for validation. A validation protocol based on 'simulated tissues' and on a list of 16 represe...

BACKGROUND AND AIM There are global public health and economic concerns on chemical residues in food of animal origin. The use of antibiotics in dairy cattle for the treatment of diseases such as mastitis has contributed to the presence of residues in dairy products. Penicillin residues as low as 1 ppb can lead to allergic reactions and shift of resistance patterns in microbial population as we...

In this study, 21 pesticides and 4 aflatoxins were monitored in baby food marketed Brazil, applying ultra-high-performance liquid chromatography coupled to quadrupole-Orbitrap mass spectrometry (UHPLC-Q-Orbitrap-MS). The quick, easy, cheap, effective, rugged, safe (QuEChERS) extraction method combined with dispersive solid-phase (d-SPE) clean-up was applied primary secondary amine (PSA), octade...

BACKGROUND The wide use of pesticides raises concerns on the health risks associated with pesticide exposure. For developing countries, like Thailand, pesticide monitoring program (in vegetables and fruits) and also the maximum residue limits (MRL) regulation have not been entirely implemented. The MRL is a product limit, not a safety limit. The MRL is the maximum concentration of a pesticide r...

background: the objective of this study was to determine the residual concentrations of ethion and imidacloprid in cucumbers grown in greenhouse. the effect of some simple processing procedures on both ethion and imidacloprid residues were also studied. methods: ten active greenhouses that produce cucumber were randomly selected. ethion and imidacloprid as the most widely used pesticides were m...

Tomato (Lycopersicum esculentum) is prominent among vegetables produced in Ghana. About ninety percent (90%) of the population of the study area are engaged primarily in tomato production. Due to the problem posed by pests and diseases and the vulnerability of vegetables to most of these pests and diseases, a variety of pesticides including organophosphates, Organochlorines, carbamates, and syn...

This study investigated the levels of the antibiotic tetracycline contained in cow milk, goat milk, butterfat, soft cheese and yoghurt samples. High performance liquid chromatography (HPLC) standard methods were used for the detection and quantification of tetracycline in 40 dairy products samples. All the analysed samples contained residues of tetracycline antibiotics. The mean tetracycline re...

In Japan, maximum residue levels (MRL) have been set for eight pesticides (a-BHC, b-BHC, g-BHC, d-BHC (BHCs), p,p′-DDE, o,p′-DDT, p,p′-DDD, p,p′-DDT (DDTs)) in 14 crude drugs (below 0.2 ppm as total of BHCs, below 0.2 ppm as total of DDTs). There are fears that pesticides present in crude drugs for which MRL are set will be changed from BHCs and DDTs to other pesticides with MRL setting as the ...