New Mg-3Zn-2Ca magnesium alloy was prepared using different processing techniques: gravity casting as well as squeeze casting in liquid and semisolid states. Materials were further thermally treated; thermal treatment of the gravity cast alloy was additionally combined with the equal channel angular pressing (ECAP). Alloy processed by the squeeze casting in liquid as well as in semisolid state ...

The effects of rare earth addition and hot extrusion process on the grain refinement of magnesium alloy were studied. The as-cast Mg-6Al-1Zn (AZ61) alloy had the average grain size of ~ 64 µm and its microstructure consisted of α-Mg and Mg17Al12 phase. By partial substitution of Al with Gd to reach Mg-4.8Gd-1.2Al-1Zn alloy, it was observed that the Mg17Al12 phase disappeared and two new interme...

A new intermetallic tetrahedrally close-packed phase, called the C phase, was found coexisting with the C14 Laves phase by means of high-resolution electron microscopy and selected-area electron diffraction. Its space group and lattice parameters are: B2/m, a = 17.8, b =7.7 , c =4 .7 ~ , ~/= 99° and Z =50 (e.s.d.'s of lattice parameters ca 0.05 A). Its atomic coordinates and orientation relatio...

It has long been known that solute segregation at crystalline defects can have profound effects on material properties. Nevertheless, quantifying the extent of solute segregation at nanoscale defects has proven challenging due to experimental limitations. A combined experimental and first-principles approach has been used to study solute segregation at extended intermetallic phases ranging from...

Determination of atomic-scale crystal structure for nanostructured intermetallic alloys, such as magnetic alloys containing Al, Ni, Co (alnico) and Fe, is crucial for understanding physical properties such as magnetism, but technically challenging due to the small interatomic distances and the similar atomic numbers. By applying energy-dispersive X-ray spectroscopy (EDS) mapping to the study of...

The aim of this work is to elucidate the formation of the amorphous phase in the Cu-Zr binary alloy system. It was found that 1 mm diameter rods with a fully amorphous structure can be prepared in a relatively wide range of compositions. In contrast, the formation of 2 mm diameter rods was achieved only for the Cu64Zr36 alloy and in the range of Cu53Zr47 Cu50Zr50, which are compositions near th...

In this work we compare the microstructures of intermetallic compounds (IMCs) in electrochemically stripped solder joints created by two different soldering methods (vapor phase soldering (VPS), and selective laser soldering with a CO2 laser). After the selective removal of the Sn phase with amperometry, the microstructure and structural composition of the IMC can be revealed in a detailed way,...

The Mg2Si intermetallic alloys have been prepared by using a powder metallurgy process. milling treatment of silicon as raw material to improve the formation phase was investigated in this research. un-milled and milled mixed with magnesium for 2 hours. powders were compacted stainless steel tubes sintered at 500 600°C 6 crystal structure identified X-ray diffractometer (XRD), while fracture su...