a fiber coating from polyaniline (pani) was electrochemically prepared and employed for solid phase micreoextraction (spme). the pani film was directly electrodeposited on the platinum wire surface using cyclic voltametry (cv) technique. the same method was applied for the preparation of spme fiber coated by polyaniline multiwalled carbon nanotubes (pani/mwcnts) composite. the concentration of ...

this study propose a new analytical protocol for the determination of benzene, xylene, toluene and styrene in water samples using homogeneous liquid-liquid microextraction via flotation assistance (hllme-fa) technique followed by gas chromatography-mass spectrometry (gc-ms). in this research, a special extraction cell was designed to facilitate collection of the low-density solvent extraction. ...

Multicomponent analyses were carried out for three types of urinary constituents: steroids, acids, and drugs and drug metabolites. The methods were based on gas-phase analytical techniques, which include the use of instruments and instrumental systems for gas chromatography, gas chromatogra phy-mass spectrometry, and mass spectrometry-com puterization. After isolating an analytical sample, we p...

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Relative to other metabolomics analysis techniques, gas chromatography mass spectrometry (GC/MS) is one of the earliest applied analysis techniques in metabolomics. The first paper on metabolomics (metabolic profiling) is derived from the application of GC/MS analysis in urine and tissue extracts (Dalgliesh et al. 1966). With the arrival of omics era and the proposing of metabolomics concept, p...

Gas chromatography coupled to mass spectrometry in negative chemical ionization (NCI) 11 mode has been applied to the quantification and reliable identification of polybrominated 12 diphenyl ethers (PBDEs) in animal and vegetable samples from aquaculture activities. 13 Matrices analyzed included fish fillet, fish feed, fish oil and linseed oil, which their fat content 14 ranged from 5 to 100%. ...