A recently constructed polyglycine modified carbon paste electrode (PGMCPE) was employed to evaluate the electrochemical behavior of methyl orange (MO). The developed electrode was characterized by FESEM to understand the morphology of the modified electrode and bare carbon paste electrode (BCPE). The modified electrode exhibits an excellent electrochemical activity towards the oxidation of MO....

Electrochemistry in combination with mass spectrometry is emerging as a versatile analytical technique in the imitation of oxidative drug metabolism during the early stages of drug discovery and development. Here, we present electrochemical O-dealkylation of phenacetin to acetaminophen by square-wave potential pulses consisting of consecutive sub-second oxidation and reduction steps. This O-dea...

This paper presents the printed thick film Ag|AgCl|KCl reference electrodes for electrochemical or biosensors application and their electrochemical and analytical performance. The reference electrode exhibits a stable potential against standard glass reference electrode with a potential difference of 5 mV in the deionized water. The anodic and cathodic peak current of the electrode increase wit...

We present a new method for developing hydrogen silsesquioxane (HSQ) by using electrical potentials and deionized water. Nested-L test structures with a pitch as small as 9 nm were developed using this electrochemical technique in saline solution without adding hydroxyl ions. Furthermore, we showed that high-resolution structures can be electrochemically developed in deionized water alone. Elec...

Copper nanoparticles were fabricated by electro-reduction of CuSO4solution in the presence of cetyltrimethylammonium bromide (CTAB) cationic surfactant as an additive through potentiostatic method. The prepared copper nanoparticles were characterized by scanning electron microscopy (SEM) and electrochemical methods. The SEM images reveal that the nanoparticles with diameters at about 70 n...

    Y-TiAl intermetallic alloy have a good potential for use as biomaterial, due to its good corrosion resistance. In this paper, two fundamental electrochemical techniques namely electrochemical impedance spectroscopy and potentiodynamic anodic polarization were used to evaluate the corrosion performance of g-TiAl in Ringer's solution. Surface modification treatments were employed with the pur...

this paper describes the development, electrochemical characterization and utilization of novel modified molybdenum (vi) complex-carbon nanotube paste electrode for the electrocatalytic determination of ascorbic acid (aa). the electrochemical profile of the proposed modified electrode was analyzed by cyclic voltammetry (cv) that showed a shift of the oxidation peak potential of aa about 235 mv ...

aisi 304l austenitic stainless steel with different grain sizes of 0.5 -12 μm was obtained through the martensiticprocess. corrosion behavior of different samples was investigated in a 0.5m hcl solution using open circuitpotential, potentiodynamic polarization and electrochemical impedance spectroscopy tests. also, the correlationbetween the grain size and pitting corrosion resistance was asses...