Nanocrystalline zinc ferrite (ZFO) has been synthesized from metal acetylacetonates by microwave irradiation for 5 min in the presence of a surfactant. The as-prepared material is ZFO and has been subjected in air to conventional furnace annealing and to rapid annealing at different temperatures. Both annealing protocols lead to well-crystallized ZFO, with crystallite sizes in the range 8–20 nm...

The proton diffusion coefficients in an electrolytic manganese dioxide (EMD) electrode at various stages of the constant current discharge have been determined by means of AC impedance technique. The finite diffusion model was applied in the numerical fitting. The crystallite size of EMD was estimated from (1 1 0), (1 2 1) and (0 2 1) diffraction peaks with both Scherrer equation and Warren–Ave...

The influence of synthesis and compaction parameters is investigated with regards to formation of high performance SrFe12O19 bulk magnets. The produced magnets consist of highly aligned, single-magnetic domain nanoplatelets of SrFe12O19. The relationship between the magnetic performance of the samples and their structural features is established through systematic characterization by Vibrating ...

The influence of wood components and cellulose crystallinity on the thermal degradation behavior of different wood species has been investigated using thermogravimetry, chemical analysis and X-ray diffraction. Four wood samples, Pinus elliottii (PIE), Eucalyptus grandis (EUG), Mezilaurus itauba (ITA) and Dipteryx odorata (DIP) were used in this study. The results showed that higher extractives ...

Nanocrystalline lead selenide (PbSe) thin films were prepared on glass substrates by a chemical bath deposition method, using sodium selenosulfate (Na(2)SeSO(3)) as a source of Se(2-) ions, and lead acetate as a source of Pb(2+) ions. Trisodium citrate (TSC) was used as a complexing agent. PbSe films were prepared at various deposition temperatures while the pH value was kept fixed at 11, and t...

The formation dynamics of medium- entropy alloy CoFeNi has been studied both experimentally and theoretically in terms molecular dynamic simulation. results experiments modelling showed good qualitative agreement supplemented each other. synthesis was found to occur two stages. (a) Refinement crystallites accumulation structural defects take place due severe plastic deformation friction metal p...

This work explores the size-induced lattice modification and its relevance to photoluminescence properties of tetragonal zircon-type GdVO(4):Eu(3+) nanostructures. GdVO(4):Eu(3+) nanoparticles with crystallite sizes ranging from 14.4 to 24.7 nm were synthesized by a hydrothermal method using sodium citrate as a capping agent. Regardless of the reaction temperatures, all samples retained an elli...

magnetic nanoparticles attracted a great deal of attention in the medical applications due to their unique properties. the most exceptional property of magnetic particles is their response to a magnetic force, and this property has been utilized in applications such as drug targeting, bioseparation, contrast agents in magnetic resonance imaging (mri) and heating mediators for cancer therapy. in...

The work is dedicated to study of thin V2O5 film formation by pen plotter printing using vanadyl alkoxyacetylacetonate as hydrolytically active precursor. Solution the prepared butoxyacetylacetonate complex with 87% butoxyl groups was used functional ink for on surface specialized chip. According atomic force microscopy (AFM) and scanning electron (SEM), oxide consists nanorods 35–75 nm in thic...