in previous studies, mebudipine, a dihydropyridine calcium channel blocker, showed a considerable potential to be used in cardiovascular diseases. the aim of the current study was to develop a valid method using reversed-phase high performance liquid chromatography coupled with electrospray ionization mass spectrometry to assay mebudipine in the human plasma. separation was achieved on a zorbax...

a column of alumina modified with sodium dodecyl sulfate (sds) and dimethylglyoxime (dmg) was prepared for the preconcentration of trace nickel from water samples for flame atomic absorption spectrometry (faas) determinations. under optimized conditions (ph=7.0; flow rate: 20 mlmin-1) nickel was retained on the column. the nickel collected on the column was eluted with 5 ml of 1 m nitric acid. ...

a clinical presentation of a metabolic disorder, often first seen in infants who present with poor feeding, vomiting, tachypnea, acidosis, hyperammonemia, ketosis, ketonuria, irritability, and convulsions or hypotonia and lethargy, findings that are otherwise suggestive of neonatal sepsis diseases with oa isovaleric and propionic acidemias, maple syrup urine disease, medium chain acyl dehydroge...

a simple, sensitive and accurate method for spectrophotometric determination of dalacinphosphatehas been established. the method is based on the reduction of atomic absorptioncalcium ion by phosphate. because, there is a phosphate mole in every dalacin mole structureand with measurement of phosphate, dalacin is beyond measurement too. therefore, the reactionbetween acidic hydrolysis products of...

Background: This study consists of two parts. The first part deals with both qualitative and quantitative analysis of 226Ra using alpha spectrometry measurement method. In the second part, the percentage of radioactive equilibrium between 226 Ra and its daughter products were determined by alpha spectrometry and total alpha measurement system after elapsed time of 15 days from precipitation. Ma...

background many members of the genus satureja have aromatic and medicinal characteristics. objectives results thymol (34.5%), γ-terpinene (18.2%) and ρ-cymene (10.5%) were the main components of the essential oil. the toxicological study on 5637 and kyse cell lines showed ic50 values of 156 μg/ml. the essential oil exhibited considerable antimicrobial activity on tested bacteria and fungi. mate...

this study was conducted to determine the radioactivity concentration in soil samples of anarak-khour district located at central iran. 48 soil samples from a depth of 10-15 cm were taken from seven different sites for monitoring. the radioactivity concentration of 238u, 232th, 137cs and 40k in soil samples was determined, using a high resolution (hpge detector, p-type) γ-spectrometry by detect...

proteomics has emerged since 1995 for studying the total proteome of cells, tissues, or organisms at any condition. the study of proteins has a fundamental importance because they are the functional and final molecules of the gene expression process and proteomics could be a valuable technique for achieving this purpose. mass spectrometry is a complementary technique for proteomics that allows ...

1. Accelerator mass spectrometry (AMS) 1.1. Reviews 1.2. AMS systems 1.3. Methodology 1.4. Developments in radiocarbon analysis 1.5. Developments in the measurement of elements other than carbon 2. Electrospray mass spectrometry (ESMS) 3. Gas chromatography-electron ionization mass spectrometry (GC-EIMS) 4. Glow discharge mass spectrometry (GDMS) 4.1. Reviews 4.2. Instrumentation 4.3. Analytica...