Sulfuric acid functionalized magnetic nanocatalyst (SAMNC) has been prepared as an efficientacidic and applied in the one-pot preparation of 2,3-dihydroquinazolin-4 (1H) -one derivatives.This catalyst has been characterized by FT-IR, SEM, and VSM. According to the obtainedresults, including time, yield and recyclability, SAMNC could be considered as an efficient catalystfor organic transformati...

1561 References Cited U.S. PATENT DOCUMENTS 3,792,423 2/1974 Becker et al. ......................... 73/620 3,979,712 9/1976 Ettenhofer et al. . 4,028,934 6/1977 Sollish ................................... 73/620 4,327,576 5/1982 Dickey et al. ................... 73/40.5 A 4,640,121 2/1987 Leuker et al. ................... 73/40.5 A 4,641,526 2/1987 Izumi et al. ........................... 73/5...

2-Dihydroquinazolin-4(1H)-thiones were prepared in up to excellent yields from 2-aminobenzothioamides and aldehydes. The reaction is carried out in water without the use of any catalyst or promoter. The sulfur-containing substrate can be obtained easily by thiation of the corresponding nitrile by solid sodium hydrosulfide.

facile and versatile procedures have been explored for the synthesis of tetrahydropyridines and 2,3-dihydroquinazolin-4(1h)-ones. these protocols employ the one-pot multi-component condensation of arylaldehydes and aromatic amines with β-keto esters and isatoic anhydride in chloroacetic acid, respectively. the reactions proceeded smoothly to generate the corresponding products in high yield. we...