A new semi-organic nonlinear optical crystal of Glycine Magnesium Chloride (GMC) has been grown by slow evaporation solution growth technique. The crystal system and lattice parameters were determined from the single crystal X-ray diffraction analysis. Fourier transform infrared (FTIR) studies confirm the various functional groups present in the grown crystal. The transmittance and absorbance o...

Abstract Prior to shoulder replacement, the quality of cancellous bone stock humerus head should be evaluated. Thermogravimetric analysis (TGA) has already been utilized assess thermal stability mineral, collected from femoral patients with osteoarthritis and osteoporosis. Our workgroup recently examined parameters rotator cuff undergoing reversed replacement. We hypothesized that TGA would ind...

Sugarcane leaves are one of the agro-industrial wastes derived from sugarcane plants. In this research, used as raw material for pyrolysis which produces three main products: liquid, solid, and gas. The focus research is to identify effect temperature on pyrolysis, mass changes, decomposition, chemical composition bio-oil. was carried out using a Circulating Fluidized Bed (CFBr) reactor with va...

The present work reports electrochemical synthesis of MgB6 from molten salts using the precursor consists of LiF-B2O3-MgCl2. An attempt has been made to synthesize metastable phase MgB6 crystal by electrolysis method. DTA/TGA studies were made to determine the eutectic point of the melt and it was found to be around 900°C. The electrolysis was performed at 900°C under argon atmosphere, at curre...

A nonlinear optical crystal of gamma glycine was grown by slow evaporation solution growth technique using deionized water and sodium acetate. The functional groups and vibrational frequencies were identified using FTIR spectral analysis. The cell parameters were determined from single crystal X-ray diffraction analysis. Thermogravimetric analysis (TGA) and differential thermal analysis (DTA) w...

The aim of this research is to synthesise carbon aerogels and to compare the differences in their textural, morphological and chemical properties when synthesised in basic and acidic media, and with two different types of pretreatment carbonization and activation with CO2. Four samples are prepared and characterised using TGA-DTA, SEM, DRX, isotherm determination of N2 adsorption-desorption at ...

A new semiorganic nonlinear optical crystal of bisthiourea nickel bromide (BTNB) was grown successfully by slow evaporation technique using water as solvent. The lattice parameters of the grown crystal have been determined by X-ray diffraction studies. Vibrational spectrum is recorded to determine symmetries of molecular vibrations. Optical absorbance spectrum recorded revealed that this crysta...

Tungstate exchanged Mg-Al layered double hydroxides as a recyclable heterogenised catalyst along with H2O2 as an oxidant for the oxidation of sec-amines to nitrones is developed for the first time, Reactions proceed at a fast rate in aqueous media in a single step at room temperature in good to excellent yields. The heterogenised catalyst showed higher activity (TOF) over their homogeneous anal...

Bismuth niobate solid solutions, BixNbOδ (2.5 ≤ x ≤ 6), have been prepared using a mechanochemical method. The solid solutions were also prepared using a solidstate conventional method for comparison purposes. Bi3NbO7 was successfully obtained via a mechanochemical method at a lower synthesis temperature (milled at 1000 rpm for one hour followed by heating at 700C for 24 h) than the conventiona...

In this research paper in air synthesis of Psyllium and zirconium(IV)tungstoiodophosphate based organo-inorganic hybrid ion exchanger has been reported. Synthesised hybrid ion exchanger has been characterized by FT-IR, SEM, EDS and TGA/DTA/DTG and chemical composition. Ion exchange capacity and thermal studies of the synthesised ion exchanger were investigated using the potassium chloride solut...