نتایج جستجو برای: xrf method

تعداد نتایج: 1632639  

Journal: :Analytical chemistry 2011
Kazuhiko Nakano Chihiro Nishi Kazunori Otsuki Yoshinori Nishiwaki Kouichi Tsuji

Micro-XRF is a significant tool for the analysis of small regions. A micro-X-ray beam can be created in the laboratory by various focusing X-ray optics. Previously, nondestructive 3D-XRF analysis had not been easy because of the high penetration of fluorescent X-rays emitted into the sample. A recently developed confocal micro-XRF technique combined with polycapillary X-ray lenses enables depth...

2016
Slávka Kaščáková Cameron M. Kewish Stéphan Rouzière Françoise Schmitt Rodolphe Sobesky Joël Poupon Christophe Sandt Bruno Francou Andrea Somogyi Didier Samuel Emmanuel Jacquemin Anne Dubart‐Kupperschmitt Tuan Huy Nguyen Dominique Bazin Jean‐Charles Duclos‐Vallée Catherine Guettier François Le Naour

Wilson's disease (WD) is a rare autosomal recessive disease due to mutations of the gene encoding the copper-transporter ATP7B. The diagnosis is hampered by the variability of symptoms induced by copper accumulation, the inconstancy of the pathognomonic signs and the absence of a reliable diagnostic test. We investigated the diagnostic potential of X-ray fluorescence (XRF) that allows quantitat...

2002
Christopher G. Worley

Two XRF specimen preparation methods were investigated for quantifying gallium in plutonium metal. Gallium in plutonium was chosen here as an example for demonstrating the efficacy of wavelength dispersive XRF for quantifying radioactive materials. The steps necessary to handle such materials safely will also be discussed. Quantification of plutonium samples by a wellestablished aqueous specime...

Journal: :Math. Program. 1988
B. R. R. Butler

X-ray fluorescence (XRF) spectrometry has been used by the oil industry since the 1950s. XRF can be found supporting activities in exploration, production, research as well as intellectual properties. Traditional applications for XRF were the analysis of single element or a limited range of multiple elements. Today, XRF encompasses high precision full spectral elemental profiles along with high...

2005
A. M. Soderberg S. R. Kulkarni E. Berger D. B. Fox P. A. Price S. A. Yost M. P. Hunt D. A. Frail R. C. Walker

We report the discovery of optical and radio afterglow emission from the extremely soft X-ray flash, XRF 020903. Our spectroscopic observations provide the first redshift for an X-ray flash, thereby setting the distance scale for these events. At z = 0.251, XRF 020903 is one of the nearest cosmic explosions ever detected, second only to the recent GRB 030329 and the unusual GRB 980425/SN 1998bw...

2003
A. M. Soderberg S. R. Kulkarni E. Berger D. B. Fox P. A. Price S. Yost M. Hunt D. A. Frail C. Walker

We report the discovery of optical and radio afterglow emission from the extremely soft X-ray flash, XRF 020903. Our spectroscopic observations provide the first redshift for an X-ray flash, thereby setting the distance scale for these events. At z = 0.251, XRF 020903 is one of the nearest cosmic explosions ever detected, second only to the recent GRB 030329 and the unusual GRB 980425/SN 1998bw...

2016
A. Shinde G. Li L. Zhou D. Guevarra S. K. Suram F. M. Toma Q. Yan J. A. Haber J. B. Neaton J. M. Gregoire

X-ray fluorescence (XRF) spectroscopy was measured on duplicate libraries deposited on Si (without BiVO4) due to the overlap between the Ce Lα line (4.839 kV) from the coating and the V Kα line (4.952 kV) from the BiVO4. The x-ray beam was approximately 2 mm in diameter. Since the XRF sampling depth far exceeds the film thickness, XRF counts for each element were assumed to be proportional to t...

2004
A. M. Soderberg S. R. Kulkarni E. Berger D. B. Fox P. A. Price M. P. Hunt D. A. Frail R. C. Walker M. Hamuy

We report the discovery of optical and radio afterglow emission from the extremely soft X-ray flash, XRF 020903. Our spectroscopic observations provide the first redshift for an X-ray flash, thereby setting the distance scale for these events. At z = 0.251, XRF 020903 is one of the nearest cosmic explosions ever detected, second only to the recent GRB 030329 and the unusual GRB 980425/SN 1998bw...

Journal: :Environmental Health Perspectives 2001
A C Todd E L Moshier S Carroll S W Casteel

The aim of this study was to apply the technique of (109)Cd-based K-shell X-ray fluorescence (XRF) bone lead measurements to swine femurs and to validate the concentrations obtained therefrom against an independent chemical measurement of bone lead: atomic absorption spectrometry (AAS). The femurs ranged in lead concentration from 1.0 to 24.5 microg of lead per gram of ashed bone, as measured b...

Journal: :Clinical chemistry 2000
T M Ambrose M Al-Lozi M G Scott

The assessment of past chronic lead exposure is difficult. Chronic lead burden is not always correctly assessed using laboratory-based tests that are useful for acute or recent exposures. We describe a case of suspected chronic lead exposure that illustrated the need for improved and possibly noninvasive methods to determine cumulative lead body burden. X-Ray fluorescence (XRF) is discussed as ...

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