This research reported a new method of removal of Pb+2from water by using a nano zero valent iron (nZVI) assisted ultrasonic wave. At first, nZVI was synthesized by an ultrasound assisted method. Particles morphology and surface composition were characterized by FESEM, XRD, and EDX. The XRD patterns showed that the crystallinity of the nZVI prepared using ultrasonic conditions was hi...

Tungsten oxide (WO3) and tungsten oxide hydrate (WO3.H2O) nanoparticles were synthesized via microwave-assisted solution combustion in comparison with the acidic precipitation method. Oxalic acid was used as a surfactant and forming agent in the acidic precipitation method. In addition to oxalic acid, glycine and citric acid were also used as fuels in the microw...

Ultrasonication has been used to accelerate chemical reactions. It would be ideal if ultrasonication-assisted chemical reactions could be monitored by suitable detection tools such as mass spectrometry in real time. It would be helpful to clarify reaction intermediates/products and to have a better understanding of reaction mechanism. In this work, we developed a system for ultrasonication-assi...

since solid-phase and liquid-phase microextraction (spme and lpme) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. however, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. in this way, in recent years, different methods such as ultrason...

This paper presents the findings on process parameters for surface roughness optimization of an open-source ultrasonic vibration assisted fused deposition modeling (FDM) printed specimen. Acrylonitrile Butadiene Styrene (ABS) material specimens and printing temperature, layer thickness, were determined as control that influenced roughness. Experimental design with Taguchi level 9 (3*3) Orthogon...

Asphaltene precipitation and deposition is a serious problem in many Iranian fields. The deposited asphaltene results in partial or total blockage of the wellbore and wellstring reducing or completely seizing oil production. This paper studies the asphaltene problem and mitigation methods in wellstring systematically. It presents new approach based on the combination of thermodynam...

In this investigation, the material removal rate, tool wear rate and surface integrity obtained by EDM, ultrasonic vibrations assisted EDM and magnetic field assisted EDM were studied and compared with together to show the quality of the effects of applying each of ultrasonic vibrations to tool and magnetic field around gap distance of EDM process on material removal rate, tool wear rate, and s...

Response surface methodology (RSM) was employed to optimize the conditions for the ultrasonic-assisted extraction (UAE) of polysaccharides from the flowers of Dendrobium devonianum. The optimal conditions for the maximum yields of DDFPs are as follows: an extraction temperature of 63.13°C, an extraction time of 53.10 min, and a water-to-raw material ratio of 22.11 mL/g. Furthermore, three fract...

The ultrasonic-aided co-precipitation method was used to create SnO2-TiO2 nanocomposite particles. Scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and UV-vis were characterize the XRD patterns revealed crystalline structure of particles average particle size determined by Debye Scherrer’s equation found be 11.355, 4.9577, 4.333 nm fo...