CaCO3 nanoparticles have been synthesized via heat-treatment of a new precursor and solid state reaction. Effect of calcinations temperature and quantity of surfactant on particle size has been investigated. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transform infrared (FT–IR) spec...

Nanocrystals of ZnO were prepared by microwave irradiation using Zn (II) acetate and triethanol amin (TEA) as the starting materials and water as solvent. The nanocrystals of ZnO with hexagonal (Wurtzite) structure were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), UV-Vis absorption and FTIR Spectroscopy techniques.

in this paper, 4,4ʹ-bipyridinium dichloride  supported sba-15 (sba@bipy2+ 2cl-) was used for the synthesis of dihydropyrimidinones. the synthesized catalyst was characterized by ft-ir spectroscopy, scanning electron microscopy (sem), transmission electron microscopy (tem) and thermogravimetric analysis (tga). this nanocomposite was shown to be an efficient heterogeneous catalyst for the synthes...

silica  coated magnetite  nanoparticles were  covalent  grafted with  3-aminopropyl trimethoxysilane  to give aptscmnps. reaction of  the resulted nanomaterial with 4-formyl benzo-12-crown-4 ether afforded fb12c4/aptsmnps  nanocomposite  material  in  which  the  crown ether  moiety  was  attached  through  propyl  chain  spacer. characterization of  the prepared nanocomposite was performed wit...

zeolite fau type-y is one of the most studied framework of all zeolites, and has been used as catalysts for number of reactions in the refinery and petrochemical industry. in this research, nanocrystalline zeolite y was synthesized by hydrothermal method. the crystal size of zeolite y is influenced by temperature, aging time, alkalinity, and water content. the synthesized zeolite nay is identif...

objective(s): cao–mgo–sio2 system bioceramics possess good characteristics for hard tissue engineering applications. the aim of the study was to synthesize the nano powder by using a sol-gel method and evaluate of bioactivity in the cells culture. methods: to characterize of powder x-ray diffraction (xrd), transmission electron microscopy (tem) and to evaluate the bioactivity sample cell seedin...

cobalt oxide (co3o4) nanoparticleshave been synthesized by hydrothermal method using mixture of cobalt(ii)chloride, triton x-100 and koh in an autoclave at 180 °c for 6 h followed by heating at 400 ºc for 3 h in air. the product have been characterized by fourier transform infrared (ft-ir), uv-vis spectroscopy, powder x-ray diffraction (xrd), scanning electron microscopy (sem) and transmission ...

in this scientific research, mno2 nanoparticles (nps) have been successfully prepared by a precipitation method using kmno4, mnso4.h2o and h2o2 (30%) as the precursors. as-prepared sample was identified by x-ray diffraction (xrd), scanning electron microscopy (sem), transmission electron microscopy (tem) and infrared (ir) techniques. the transmission electron microscopy (tem) showed 7-8 nm rang...

In transmission electron microscopy (TEM) for biological and polymer samples, it is difficult to image with high contrast, since they are mostly composed of light elements and have similar density. One solution to enhance the contrast is utilization of phase contrast microscopy, which is realized in optical microscopy. Accordingly, many types of phase plates for electron microscopy have been pr...

Real-time electron microscopy observations of processes in wet environments, i.e., solutions, liquids, etc. have become possible only very recently with the development of electron beam transparent cells, in which a liquid layer is trapped between two ultrathin, electron-transparent membranes. Liquid-cell transmission electron microscopy (TEM) and scanning TEM (STEM) have attracted a lot of int...