Abstract Through the functional disassembly study of pressurization system, vacuum and atmosphere control water cooling system SPS spark plasma equipment, problems in actual production process corresponding improvements sintering (SPS) equipment are also discussed. The shortcomings its development directions proposed to provide sufficient data support for subsequent research.

The Si-coated SiC (Si-SiC) composite nanoparticle was prepared by non-transferred arc thermal plasma processing of solid-state synthesized SiC powder and was used as a sintering additive for SiC ceramic formation. Sintered SiC pellet was prepared by spark plasma sintering (SPS) process, and the effect of nano-sized Si-SiC composite particles on the sintering behavior of micron-sized SiC powder ...

Spark plasma sintering (SPS) is currently widely applied to existing alloys as a means of further enhancing the alloys' figure of merit. However, the determination of the optimal sintering condition is challenging in the SPS process. This report demonstrates a systematic way to independently optimize the Seebeck coefficient S and the ratio of electrical to thermal conductivity (σ/κ) and thus ac...

Si2N2O is considered as a new great potential structural/functional candidate in place of Si3N4. The amorphous Si3N4 nanopowder was incorporated into silica sol by adding of MgO and Y2O3 as sintering aid. Synthesized powders were heated by spark plasma sintering at a heating rate of 100 oC/min yielded fully dense compacts at 1550 and 1750 oC for 40 min. The phase formation of samples was charac...

TaC and HfC are thought to have the highest melting point (~4000°C) among all refractory materials. The binary solid solution of TaC and HfC (Ta4HfC5) is also considered as the most refractory material with the melting point over 4000 °C and valuable physical and mechanical properties. The main goal of this work is to fabricate TaC/HfCbased composites which consolidated by means of spark plasma...

In this research study, the effects of aluminum nitride (AlN) additive on the densification behavior and microstructure development of titanium diboride (TiB2) based ceramic matrix composite were investigated. In this way, a monolithic TiB2 ceramic and a TiB2–5 wt% AlN ultrahigh temperature ceramic composite were fabricated by spark plasma sintering (SPS) proces...

It is known that work pieces with nanocrystalline structure condition have much higher performance than those with an ordinary structure. There are known number of techniques for manufacturing of nanocrystalline materials in powder condition however a question of manufacturing bulk pieces in the same nanocrystalline state mentioned is that compaction and synthesizing of nanocrystalline powders ...

Data regarding bulk polycrystalline nickel samples obtained by powder metallurgy using Spark Plasma Sintering (SPS) are presented, with a special emphasis on the influence of a cold isostatic pre-compaction on the resulting morphologies and subsequent mechanical properties. Three types of initial powders are used, nanometric powders, micrometric powders and a mixture of the formers. For each ty...

In the present work, the processing and characterization of electroconductive Alumina-TiC-Ni nanocomposites obtained by Spark Plasma Sintering (SPS) are described. These nanocomposites are singular due to the excellent mechanical properties they present (particular regarding Vickers hardness, 25.6 ± 0.7 GPa), as well as their extremely good wear behaviour, studied under “ball-on-disk” dry slidi...