Two solution-based methods, metallo-organic decomposition and sol–gel processes, were used to study the effects of precursor solution type on the microstructure evolution and texture development of oriented PZT films. Microstructure development and perovskite content are strongly dependent on the heating rate. Fast heating rate forms a dense fine-grained microstructure with (111) orientation. I...

Se describen tres métodos para obtener hidroxiapatita (HA). La HA es una cerámica muy interesante por sus múltiples aplicaciones médicas. Los primeros dos métodos de precipitación parten de compuestos de calcio y fósforo, mientras que el tercer método es un proceso sol-gel que usa alcóxidos. Los productos fueron caracterizados y comparados entre sı́. Las diferencias observadas son importantes pa...

Development of optical biosensors is an active area of research in the field of medical technology. Sol-gel matrices made from alkoxide silicates, tetraethyl orthosilicate (TEOS) appear to be suitable glassy host matrix for the sensing system. However, the major problem in the TEOS based sol-gel matrices is stability. So it is important to study dopant-matrix interaction as a function of time. ...

Ridge and buried channel waveguides were fabricated on different substrates such as SiO2-on-Si, Si, glass wafers and Printed Circuit Boards by a sol-gel processing together with a photolithography process using photopatternable hybrid sol-gel materials. Thick sol-gel films of up to 100 microns were developed using a modified sol-gel process and ridge waveguides with vertical smooth sidewalls we...

Sol-gel derived silica possess many promising features, including low-temperature preparation procedure, porosity, chemical and physical stability. Applications exploiting porous materials to encapsulate sensor molecules, enzymes and many other compounds, are developing rapidly. In this paper some potential applications, with emphasis on biomedical and environmental ones, are reviewed. The mate...

This work presents a novel method for direct desorption/ ionization of analytes from sol-gel-derived film. 2,5-Dihydroxy benzoic acid (DHB), a common MALDI matrix, was incorporated into a sol-gel polymeric structure. The sol-gel-derived DHB thin film can assist the mass analysis of analytes by laser desorption/ionization, with a matrix interference-free background in the mass spectra. The sol-g...

sol-gel and polymeric membrane electrodes, based on thiacalix[4]arene as a neutral carrier, weresuccessfully developed for the detection of vo2+ in aqueous solutions. the sol-gel and pvcmembrane electrodes exhibited linear response with nernstian slopes of 29.3 and 28.4 mv perdecade, respectively, within the vanadyl ion concentration ranges from 1.0 × 10-6 to 1.0 × 10-1mol dm-3 and from 1.0 × 1...

in this research zinc oxide (zno) nano-crystalline powders were prepared by sol-gel method using zinc acetate. the zno nanoparticles were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), ultraviolet-visible (uv-vis), fourier transform infra-red (ft-ir) and energy dispersive x-ray (edx) spectroscopy. the structure of nanoparticles was studied using xrd pattern. the c...

beryllium  oxide  (beo)  nanopowder  was  synthesized  using  sol-gel method  and  the  effects  of  changes of  chemical  reagents  were investigated.  because  of  tissue  equivalence  and  other  outstanding thermoluminescence  (tl) properties of  the bulk material  in x and γ dosimetry, the applicability of this nanostructure in tl dosimetry was studied  following  irradiation to  the 137 c...

Recent developments in the preparation of surfactant-templated mesostructured sol-gel silica materials have extended the morphology from the originally discovered powders, with particle sizes on the order of microns, to mesoporous continuous thin films. These films could find applications in membrane-based separations, selective catalysis and sensors. Particularly, sodium dodecyl sulfate (SDS)t...