نتایج جستجو برای: sol gel method and xrd technique
تعداد نتایج: 17121661 فیلتر نتایج به سال:
In the organic field effect transistors (OFETs) generation, the silicon gate oxide is 1-2 nm thick. A shrinking of this thickness down to less than 1 nm for the next generation will led to a couple of orders of magnitude increase in tunnelling as well as leakage currents. NiO-SiO2 can be used in a variety of devices, such as in circuit boards and detectors, including sensors, due to its porous ...
The polycrystalline SrTiO3 thin films were prepared by the sol-gel-hydrothermal method on glass substrates. synthesis pathway was initiated preparing a clear TiO2 solution using sol-gel method. This then deposited substrate dip coating technique, followed transformation of layer into hydrothermal crystal structure, bond interactions, and band gap energy layers characterized X-ray Diffraction (X...
The powders of Ba(Ce1-xZrx)0.90Y0.1O3-δ (BCZY) with 0.2 ≤ x ≤ 0.6 have been prepared by a modified sol-gel method. Triethylenetetramine (TETA) was employed as chelating agent. Phase formation of calcined powders at 1100C and sintered pellets at 1400C of BCZY were examined by an X-ray diffractrometer (XRD). XRD results showed the calcined powder and sintered pellet formed a single perovskite pha...
zno thin films with preferred orientation along the (002) plane were prepared onto the glass substrates by the sol-gel spin coating method for different post- annealing temperatures. the xrd study confirms that the thin films grown by this method have good crystalline hexagonal wurtzite structure. the optical band gap of the samples was determined from uv-visible spectra. it is found that the s...
the preparation of nano-sized tio2 by titanium tetraisopropoxide (ti(oipr)4) via sol-gelmethod using acid as a catalyst is investigated and the optimized conditions concerning theproportional amount of acid, water, alcohol is established by xrd and sem. the effect ofcalcination temperature on phase transformation of tio2 (rutile, anatase and brookite) wasdetermined by xrd. the smallest grain si...
objective(s): cao–mgo–sio2 system bioceramics possess good characteristics for hard tissue engineering applications. the aim of the study was to synthesize the nano powder by using a sol-gel method and evaluate of bioactivity in the cells culture. methods: to characterize of powder x-ray diffraction (xrd), transmission electron microscopy (tem) and to evaluate the bioactivity sample cell seedin...
nanostructured alumina thin films were coated on stainless steel by sol-gel dip coating method. in order to prevent crack formation, al2o3 films were kept in a solvent bath immediately after coating to reduce the rate of drying. effects of calcination temperature and withdrawal speed on structural properties were analyzed using xrd and sem. topography and thickness of coatings were analyzed by ...
We fabricated YBa2Cu3-xMxO7- d (M=Ni, Fe) bulk samples, with stochiometric amount 0≤x≤0.045 by sol-gel method. The phase analysis and microstructure of specimens were examined by XRD and SEM. The electrical resistivity was measured using standard four probe technique for 77-300K. Investigation of XRD spectrum by MAUD shows Ni and Fe ions substitute in Cu(2) and Cu(1) site, respectively. Transi...
heteropoly acid promoted nanoparticle of nickel oxide samples were prepared by sol-gel method using heteropoly acids. prepared composite was characterized by xrd, ft-ir and icp technique. in this work, we have reported bromination of phenol, its derivatives and some aromatic compounds. the liquid phase bromination of phenol was performed using heteropoly acids immobilized nanoparticle of nickel...
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