Pulsed column experiments using Co, fulvic acid and porous sediment packing, along with up/down-flooding experiments using Eu, humic acid and intact sandstone blocks have been performed. The elution of metal and humic and their distribution along the sandstone columns have been measured. A mixed equilibrium and kinetic coupled chemical transport model has been used to simulate the results. In b...

A programmed temperature vaporizer (PTV) injection technique has been recently implemented in our laboratory. In present paper its performance is compared with other GC injection techniques commonly used in trace analysis of organic contaminants. Twenty-six pesticides representing different chemical classes were selected for the study. This group comprised compounds typically subjected to discr...

We report the first demonstration of soft x-ray amplification in an elongated plasma column produced by laser irradiation of a gas puff target. The gas puff target is formed by the pulsed injection of gas from a high-pressure solenoid valve through a nozzle in the form of a narrow slit. The plasma column to be used as an x-ray laser active medium is produced by irradiating the gas puff target w...

A novel detection method for the cardiac glycosides digitoxin, digoxin, and their metabolites is described. Both isocratic and gradient water-acetonitrile elutions were employed with an octadecylsilane column. The effluent was monitored by integrated pulsed amperometry in an alkaline medium (pH> 12) by adding sodium hydroxide post-column. Using isocratic elution, peak responses were linear from...

We report a case of rapidly progressive interstitial pneumonia associated with clinically amyopathic dermatomyositis who responded to single course of polymyxin b-immobilized fiber column treatment. Initial treatment with pulsed corticosteroids and cyclophosphamide, intravenous immunoglobulin, and cyclosporine seemed to suppress the activity of interstitial lung disease temporarily, but signs o...

Holdup was measured at various frequencies, amplitudes, continuous and dispersed phase flow rates for binary systems in a pulsed plate column capable of providing samples at various heights. The binary systems was so selected as to cover a wide spectrum of interfacial tensions. Dispersed phase holdup was found to increase with height in a logarithmic fashion at conditions away from the flooding...