we report on the synthesis, morphology, chemically and structurally of tio2-nio-sio2 nanostructure. the tio2-nio-sio2 nanostructure was synthesized by a method based on the sol-gel method, by the simultaneous gelation of all cations. the coatings were deposited on dried soda-lime glass slides by spin coating. composite powders and coating on glass have been characterized by xrd, sem, edax, and ...