INTRODUCTION To improve the fracture resistance of nickel-titanium (NiTi) files, manufacturers have introduced new alloys and developed new manufacturing processes for the fabrication of NiTi files. This study aimed to examine the phase transformation behavior and microstructure of NiTi instruments from a novel controlled memory NiTi wire (CM wire). METHODS Instruments of EndoSequence (ES), P...

A new powder metallurgy technique for creating porous NiTi is demonstrated, combining liquid phase sintering of prealloyed NiTi powders by Nb additions and pore creation by NaCl space-holders. The resulting foams exhibit well-densified NiTi–Nb walls surrounding interconnected pores created by the space-holder, with controlled fraction, size, and shape. Only small amounts of Nb (3 at.%) are need...

Functionally graded NiTi structures benefit from the combination of the smart properties of NiTi and those of functionally graded structures. This article provides experimental data for thermomechanical deformation behaviour of microstructurally graded, compositionally graded and geometrically graded NiTi alloy components, related to the research article entitled "Functionally graded shape memo...

NiTi wires were brazed together via eutectic reaction between NiTi and Nb powder deposited at the wire contact region. Phase transformation and deformation behavior of the NiTi-Nb eutectic microstructure were investigated using transmission electron microscopy (TEM) and cyclic loading-unloading tests. Results show that R phase and B19' martensite transformation are induced by plastic deformatio...

Surface nanomechanical behavior under nanoindentation of ZrN and ZrCN film on NiTi substrate was studied. The surface hardness and modulus of the films increase initially with larger nanoindentation depths and then reach their maximum values. Afterwards, they diminish gradually and finally reaching plateau values which are the composite modulus and composite hardness derived from the ZrN/ZrCN f...

OBJECTIVE To analyze the effect of various coating formulations on the mechanical and corrosion properties of nickel-titanium (NiTi) orthodontic wires. MATERIALS AND METHODS Uncoated, rhodium-coated, and nitrified NiTi wires were observed with a three-point-bend test, surface roughness (Ra) measurement, scanning electron microscopy, energy dispersive spectroscopy, and electrochemical testing ...

BACKGROUND It has been demonstrated that fluoride prophylactic agents may cause hydrogen absorption in NiTi wires and degrade their mechanical properties. AIMS To investigate the effect of a fluoride mouthwash on load-deflection characteristics of three types of nickel-titanium-based orthodontic archwires. METHODS Twenty maxillary 0.016 inch round specimens from each of the single-strand Ni...

BACKGROUND and Overview. With the increased use of nickel-titanium (NiTi) rotary instruments for root canal preparation in endodontics, instrument fracture has become more prevalent. Extensive research has been conducted on the physical properties and mechanical characteristics of NiTi rotary instruments, as well as the factors that can contribute to instrument failure. NiTi rotary instruments ...

The electrochemical corrosion behavior of NiTi alloy electrodeposited conductive polypyrrole (PPy) coatings doped with small size sulfate (SO42 ), medium size para-toluene sulfonate (pTS ) and large size dodecylbenzene sulfonate (DBS ) counter anions has been studied by electrochemical measurements and surface analysis. It is demonstrated that PPy coatings inhibit the corrosion of NiTi substrat...

Porous NiTi with an average porosity of 55 vol % and a general pore size of 100-600 microm was synthesized by self-propagating high temperature synthesis (SHS) with the addition of mechanically alloyed nanocrystalline Ni-Ti as the reaction agent. The SHS of porous NiTi using elemental powders was also performed for comparison. To enhance the bioactivity of the metal surface, porous NiTi synthes...