the synthesis of nanocrystalline fe3al powder by mechanical alloying as well as the structural ordering of the synthesized fe3al particles during the subsequent thermal analysis were investigated. mechanical alloying was performed up to 100 hours using a planetary ball mill apparatus with rotational speed of 300 rpm under argon atmosphere at ambient temperature. the synthesized powders were cha...

PURPOSE To measure the surface loss of dental restorative zirconia and the short-term bond strength between an indirect composite resin (ICR) and zirconia ceramic after various sandblasting processes. MATERIALS AND METHODS Three hundred zirconia bars were randomly divided into 25 groups according to the type of sandblasting performed with pressures of 0.1, 0.2, 0.4 and 0.6 MPa, sandblasting t...

Simultaneous application of colloidal processing and liquidforming additives to alumina resulted in a sintered density of >99% in 1 h at a temperature as low as 1070°C for a commercial high-purity alumina powder at a total dopant level of 2 mol%. The additives were 0.9% CuO + 0.9% TiOz + 0.1% B 2 0 3 + 0.1% MgO. At higher temperatures or after prolonged sintering, the doped alumina ceramic deve...

Abstract Nanocrystalline boehmite material was synthesized using the hydrothermal method. Different annealing temperatures have been used to transform into different alumina phases study effect of phase transitions on thermoluminescence properties alumina. XRD analysis carried out investigate crystal structure phases. The glow curves for showed structures; however, sensitivity almost constant a...

Nanocrystalline ceria has been synthesized by a non-hydrolytic method using organic solvent and precipitant. The effect of the source compound on final nanocrystalline powder was investigated. The cerium nitrate hexahydrate subjected to different vacuum/thermal treatments to get cerium source compound having different extent of water of crystallization. The nanoceria, synthesized from these com...

The paper reports a process for synthesis of γ-alumina from kaolin. Kaolin was transformed to meta-kaolin by calcination at 800 ̊C for 2h. γ-alumina powder was synthesized through extracting alumina from metakaolin via H2SO4 and meta-kaolin reactions and consequently precipitation in ethanol, which led to form the aluminum sulfate. The precipitated aluminum sulfate was dried and calcined at 900 ̊...

Single crystalline BaTiO3 (BT) was prepared using TiCl4, BaCl2 and oxalic acid. The structure of the prepared nanocrystalline BT powders were a tetragonal perovskite according to XRD and HRTEM analysis. Annealing powder to 750C show that pure BT phase was formed according to XRD, TG, and FTIR spectroscopy. The TEM images of the prepared powder reveal spherical morphology of BT, while a finger t...

Hydroxyapatite/alpha-alumina composites were prepared by means of high-energy vibratory ball milling. The effect of the addition of alumina, from 5 to 25 wt%, was investigated. x-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR) results indicated thathydroxyapatite andaluminawere themajorphases aftermechanicalmilling and only small peak shifts were observed. Transmission...

Powder formation in silane plasmas has been considered as a technology drawback because it might lead to the formation of macroscopic defects in the deposited layers. Here we summarize our recent efforts in controlling the formation of powder precursors, in particular, nanocrystalline silicon particles, aiming at their incorporation in the films. Indeed, the incorporation of clusters and crysta...

Structural changes during the deformation-induced synthesis of nanocrystalline Fe-10Cr-3Al alloy powder via high-energy ball milling followed by annealing and rapid consolidation by spark plasma sintering were investigated. Reduction in crystallite size was observed during the synthesis, which was associated with the lattice expansion and rise in dislocation density, reflecting the generation o...