Three methods (using GM3 quantities ranging from a few milligrams to grams) have been developed to prepare, in high yield, the three derivatives of ganglioside GM3 [alpha-Neu5Ac-(2-3)-beta-Gal-(1-4)-beta-Glc-(1-1)-ceramide]: deacetyl-GM3 [alpha-Neu-(2-3)-beta-Gal-(1-4)-beta-Glc-(1-1)-ceramide], lyso-GM3 [alpha-Neu5Ac-(2-3)-beta-Gal-(1-4)-beta-Glc-(1-1)-sphingosine], and deacetyl-lyso-GM3 [alpha...

Oils with high content of free fatty acid (FFA) can be treated by acid esterification where an alcohol reacts with the given oil in the presence of acid catalyst. The investigated parameters include methanol to oil ratio, temperature and amount of catalyst. The optimum conditions for acid esterification which could reduce FFA content in the feedstock to less than 1.88% (acid value 3.76 mg KOH/g...

Anisotropic wet etching is a most widely employed for the fabrication of MEMS/NEMS structures using silicon bulk micromachining. The use of Si{110} in MEMS is inevitable when a microstructure with vertical sidewall is to be fabricated using wet anisotropic etching. In most commonly employed etchants (i.e. TMAH and KOH), potassium hydroxide (KOH) exhibits higher etch rate and provides improved a...

Optimization studies for the esterification and transesterification of oil extracted from Croton gratissimus grains were carried out using response surface methodology (RMS) that utilizes central composite design (CCD) analysis variance (ANOVA). A 2 3 full-factorial rotatable CCD three independent variables at five levels was developed in each case, giving a total 20 experiments needed per stud...

This study was carried out to synthesize 1D inorganic nanostructure using an electrochemical method without any template and additives. Copper foils were anodized in a KOH bath and were tested for their antibacterial performance. After anodizing, the obtained samples were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD) to determine the corresponding morphology an...

This work aims to identify a suitable electrolyte composition for the operation of zinc–nickel flow cell at ambient temperature. The effect varying containing KOH, ZnO, tetraethylammonium hydroxide (TEAH) or tetrabutylammonium bromide (TEAB) additives are investigated. A 15 mM concentration TEAH is found provide smooth and compact zinc depositions. Increasing concentrations KOH be detrimental v...

The electroreduction of CO2 to C1-C2 chemicals can be a potential strategy for utilizing CO2 as a carbon feedstock. In this work, we investigate the effect of electrolytes on the electroreduction of CO2 to CO on Ag based gas diffusion electrodes. Electrolyte concentration was found to play a major role in the process for the electrolytes (KOH, KCl, and KHCO3) studied here. Several fold improvem...

This paper presents the preparation of in situ electrodeposited rGO/MnO2 nanocomposite as a binder-free electrode for supercapacitor application. The work describes and evaluates the performance of prepared electrode via green and facile electrodeposition technique of in situ rGO/MnO2-glucose carbon nanocomposites. The carbon content in the composite electrode increased after GO and D (+) gluco...