نتایج جستجو برای: hydrothermal process
تعداد نتایج: 1326923 فیلتر نتایج به سال:
Porous CdSe nanorods having a novel flute-like morphology have been prepared facilely via the hydrothermal treatment of CdSe·(en)0.5 (en = ethylenediamine) nanorods as sacrificial templates. During the hydrothermal process, various crystalline imperfections such as stacking faults and twinning planes appear due to lattice mismatches between orthorhombic CdSe·(en)0.5 and hexagonal wurtzite porou...
Cu2ZnSnS4 (CZTS) hierarchical microstructures were synthesized by using a facile and nontoxic hydrothermal route, which were characterized by X-ray powder diffraction (XRD), scanning electron microscope (SEM), Raman spectra, and UV-Vis absorption spectra. The results and analysis show that surfactants used in the hydrothermal process have significant effect on the phase structures, morphologies...
In this study, carbon nano-micro spheres with tightly controllable size, regular and perfect shape, high yields and narrow size distribution were prepared simply from glucose and DI water as precursors using a hydrothermal method. By setting the initial concentration of glucose solution and changing the hydrothermal process time at a constant temperature of 160 °C, carbon spheres with various s...
Citrate was used as chelating or morphology regulating agent in this study. In the presence of regulating agent a two-dimensional monetite phase evolved into three-dimentional hydroxyapatite microspheres with an average diameter of 4 µm. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) studies revealed the importance of Ca/citrate ratio in regulating the particle m...
In this research, a single-stage low-temperature hydrothermal synthesis route was successfully developed for preparation of Iron Disulfide. The prepared powder was characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). These analyses showed that nanoparticles were well crystallized, pyrite was the main product and the shape of crystals was nanorod. Also, the influences...
A simple and effective route to improve the fluorescence of carbon dots is reported. A weak fluorescent solution was obtained by a diminution step to obtain tiny particles from bagasse-based carbonaceous blocks. This solution was subjected to hydrothermal treatment under alkaline conditions to improve its fluorescent performance. The luminescence was found to be improved by more than 20-fold af...
The term “hydrothermal” comes originally from the field of geology. Hydrothermal reactions generally can be defined as reactions in the presence of aqueous solvents under high temperature and pressure. Such reactions played a very important role during formation of fossil fuels. On the basis of the natural phenomena, we have conducted a series of studies concerning hydrothermal conversion of bi...
In this paper, we report the combination of atomic layer deposition (ALD) with hydrothermal techniques to deposit ZnO on electrospun polyamide 6 (PA 6) nanofiber (NF) surface in the purpose of antibacterial application. The micro- and nanostructures of the hierarchical fibers are characterized by field emission scanning electron microscopy (FE-SEM), high-resolution transmission electron microsc...
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