JP-8, a surrogate fuel, and several model compounds were used to produce soot aerosols in a drop-tube furnace with optical access. The soluble organic fractions (SOF) of soot aerosols were studied with GC, GC-MS, and 13C NMR. The residue of each aerosol sample was studied with Raman spectroscopy, ESR, and a recently developed technique used to determine the conductivity and extent of turbostrat...

Direct determination of tin in human hair was performed by graphite furnace atomic absorption spectrometry. Human hair was cut into 3-5 mm long and 1-2 mg of the sample was directly introduced into a pyrolytically coated graphite tube, of which the injection hole was enlarged to a diameter of approximately 5 mm. After introduction of the sample, 20 μl of 30 mg Pd/l in 1 mol/l HCl was added as a...

A high temperature combustion method was used to analyze the 14C and 3H activities in graphite and the dose assessment was carried out to determine the clearance in the conservative way. By this method, the 3H and 14C were simultaneously trapped in the nitric acid and carbosorb, respectively. Accordingly, the sample preparation time for the measurement was reduced to the half. The combustion te...

The booming Asian economies are driving the recent increase in steel production. Although BOF steel production growth is much stronger than EAF, the outlook for EAF is promising due to increasing substitution of steel scrap by DRI and pig iron, as well as an increase in electrical energy supply in China. The favorable operational reliability of AC-furnaces is the reason that most new furnace pr...

This Horizontal Standard includes principles and procedures for the determination of trace metals in aqua regia and nitric acid digests of sludge, soil and treated biowaste and neighbouring samples, using atomic absorption spectrometry with electrothermal atomization in a graphite furnace. The method is applicable for determination of low concentrations of the following elements: Ag, Cd, Co, Cr...

thallium is widely found in nature, but the only inorganic stones full of this element are crookesite and lorandit. it isalso found in pyrites of copper, lead and inorganic stones. the element and its compositions are toxic and harmful to theenvironment; therefore, its application requires caution and further research. it is important to develop sensitive andaccurate analytical methods to deter...

In order to discuss the matrix modifier effect of palladium, iron, and a mixture of palladium and iron for the determination of cadmium in graphite-furnace atomic absorption spectrometry (GF-AAS), we measured the absorption profiles of a cadmium line at various compositions of these elements. Variations in the gas temperature were also estimated with the progress of atomization, by using a two-...

The melting temperatures have been determined for a wide range of substances as a function of pressure. In the present work, Teflon (polytetrafluoroethylene) was investigated up to 30 kb and the decomposition temperatures, and the melting temperatures of silver chloride and iodine were determined up to 30 kb and 20 kb, respectively. General Technique. -The pressure was generated with a piston-c...

In this article, we determined the concentration levels of metals including Zn, Al, Sr, and Co and metalloid of As of ballast water in commercial ships entering Bushehr port, along the Persian Gulf. Ballast water samples were taken from commercial ships entering Bushehr port from 34 ports around the world during 15 February and 25 August 2016. The concentration levels of metals and metalloid we...

The monitoring of trace metals in human urine plays an important role in research. Traditionally, urine analysis has been accomplished by graphite furnace atomic absorption (GFAA). However, when large numbers of samples are analyzed for multiple elements, GFAA becomes very cumbersome and restrictive, since it can only determine one element at a time. Additionally, the detection capability of IC...